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Green organic chemistry: strategies, tools, and laboratory experiments.

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Green Organic Chemistry: Strategies, Tools, and Laboratory Experiments 1st Edition

• ISBN-10 0534388515
• ISBN-13 978-0534388515
• Edition 1st
• Publisher Cengage Learning
• Publication date May 7, 2003
• Language English
• Dimensions 8.38 x 0.58 x 10.88 inches
• Print length 256 pages
• See all details

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• Publisher ‏ : ‎ Cengage Learning; 1st edition (May 7, 2003)
• Language ‏ : ‎ English
• Paperback ‏ : ‎ 256 pages
• ISBN-10 ‏ : ‎ 0534388515
• ISBN-13 ‏ : ‎ 978-0534388515
• Item Weight ‏ : ‎ 1.32 pounds
• Dimensions ‏ : ‎ 8.38 x 0.58 x 10.88 inches
• #683 in Organic Chemistry (Books)
• #2,054 in Chemistry (Books)
• #15,302 in Education (Books)

About the author

Kenneth m. doxsee.

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Green Chemistry

Green Chemistry is the utilization of a set of principles that reduces or eliminates the use or generation of hazardous substances in the design, manufacture, and application of chemical products.

Green Chemistry Initiatives

Safe & Sustainable Labs Program

The Safe & Sustainable Labs Program (previously known as Green Labs) promotes labs to operate in a more sustainable way. Extensive efforts are focused on reduction of energy use. These include hibernating  fume hoods, shutting the fume hood sash, and assessing electrical energy use. Review the  “How to be a Green Lab at MIT” web course (Atlas Learning Center) for recommendations and techniques to conserve energy and resources.

Pollution Prevention (P2)

Pollution prevention (P2) is the practice of reducing or eliminating the generation of waste while avoiding shifting the hazards from one medium to another (e.g., from water to air, from hazardous waste to solid waste, or from environmental concerns to fire safety concerns).

MIT Pollution-Prevention (P2) Program  includes silver recovery, ethidium bromide substitution and solvent recycling.

Chemical Inventory

Promotes the culture of keeping a good inventory . The EHS Office offers Environmental Health & Safety Assistant (EHSA) , an easy to use, streamlined user interface chemical inventory system. With a well-maintained chemical inventory, over-purchasing will be reduced, leading to less chemical waste.

Chemical Sharing/Exchange

Encourages chemical sharing and exchange leading to reduction or elimination of unnecessary purchases, thereby minimizing chemical waste.

• EHSA facilitates chemical sharing by allowing users to search chemical inventories within their department(s) for specific chemicals being shared by other labs.
• EHS Office coordinates chemical exchange whereby chemical users post their unwanted, preferably unopened chemicals that would otherwise be disposed for use by others who could use them. Chemical exchange between users saves time and money on both ends, removing unwanted chemicals without incurring disposal costs for one lab while providing other labs with the opportunity to acquire chemicals without incurring purchasing costs.

Note: The chemical exchange SOG will be published and linked here in the future.

How to Make Your Chemistry Greener?

• Participate in the MIT’s green chemistry initiatives. Contact your DLC EHS Coordinator or the EHS Office to learn more about how to implement these initiatives in your work process.
• Prior to purchasing new chemicals, review your lab’s current chemical inventory/search the shared inventory . When purchasing new chemicals, purchase the minimum quantities of commercial chemicals necessary for your work. Offer surplus that is in good conditions to other potential users instead of disposing it.
• Consider substituting chemicals with greener alternatives. Refer to the Resources/Tools for Green Alternatives (see below) for more information. Check with manufacturers for greener alternatives.
• Design work process with Green Chemistry’s 12 Principles. Attain the highest level of the pollution-prevention hierarchy by reducing pollution at its source.
• Design or modify your chemical experiment to make it more environmentally friendly and sustainable. Consider waste and hazard prevention during design, rather than disposing, treating, and handling waste after the experiments.

Examples of Green Experimental Procedures

• Reduce of the volume of waste and by-products that are generated during each step of synthesis.
• Eliminate use of toxic reagents and solvents.
• Mechanochemistry – solvent free, ambient temperature and increased atom economy.
• Replace solvents by their green alternatives such as water, supercritical fluids, ionic liquids, etc.
• Use of catalysts.
• Conduct the experiments at, or closer to, ambient temperatures and pressures.
• Replace traditional heating of the reaction mixture with alternative energy sources such as photochemical, microwave or ultrasonic irradiation.

12 Principles of Green Chemistry

1. Prevent Waste

Design chemical syntheses to prevent waste. Leave no waste to treat or clean up.

2. Maximize atom economy

Design syntheses so that the final product contains the maximum proportion of the starting materials. Waste few or no atoms.

3. Design less hazardous chemical syntheses

Design syntheses to use and generate substances with little or no toxicity to either humans or the environment.

4. Design safer chemicals and products

Design chemical products that are fully effective yet have little or no toxicity.

5. Use safer solvents and reaction conditions

Avoid using solvents, separation agents, or other auxiliary chemicals. If you must use these chemicals, use safer ones.

6. Increase energy efficiency

Run chemical reactions at room temperature and pressure whenever possible.

7. Use renewable feedstocks

Use starting materials (also known as feedstocks) that are renewable rather than depletable. The source of renewable feedstocks is often agricultural products or the wastes of other processes; the source of depletable feedstocks is often fossil fuels (petroleum, natural gas, or coal) or mining operations.

8. Avoid chemical derivatives

Avoid using blocking or protecting groups, or any temporary modifications if possible. Derivatives use additional reagents and generate waste.

9. Use catalysts, not stoichiometric reagents

Minimize waste by using catalytic reactions. Catalysts are effective in small amounts and can carry out a single reaction many times. They are preferable to stoichiometric reagents, which are used in excess and carry out a reaction only once.

10. Design chemicals and products to degrade after use

Design chemical products to break down to innocuous substances after use so that they do not accumulate in the environment.

11. Analyze in real-time to prevent pollution

Include in-process, real-time monitoring, and control during syntheses to minimize or eliminate the formation of byproducts.

12. Minimize the potential for accidents

Design chemicals and their physical forms (solid, liquid, or gas) to minimize the potential for chemical accidents, including explosions, fires, and releases to the environment.

Resources/Tools for Green Alternatives

Check out the information below for examples of how to apply the 12 Principles of Green Chemicals to chemical reactions. Evaluate your experiments with Millipore-Sigma DOZN TM Tool to see how green they are.

Solvent selection is a key priority in greening chemistry because solvents are used in high volumes and many of them are flammable and toxic compounds. Their usage creates large amounts of waste, air and water pollution, and other health and environmental impacts. Consider green alternative solvents with low toxicity, minimal safety concerns, and little impact on the environment to make a greener process or product.

Interested to have a solvent selection guide at your lab? Download the Green Chemistry Guide and request a Greener Solvent Guide magnet from Beyond Benign .

Solvent Selection Guide for Laboratory Scale

Several solvent selection guides have been developed by pharmaceutical industries for the small-scale chemistry laboratories. Table 1 shows a simple solvent selection guide developed by Pfizer . The solvents are assessed based on safety, health, environment, and regulatory criteria and categorized as preferred, usable, and undesirable.  If you plan to use the undesirable solvents, consider using the suggested alternatives in Table 2. Check out the solvent selection guides developed by GSK , Sanofi and   AstraZeneca and unified solvent selection guides for common solvents used in medicinal chemistry.

Table 1: Solvent selection guide developed by Pfizer

Reference: Green Chemistry , 2008, 10, 31

Table 2: Suggested alternatives for undesirable solvent

*If a chlorinated solvent needs to be used, dichloromethane is the best choice out of the four.

**All the solvents have good replacements, except for one group, which is the dipolar aprotic solvents (dimethyl formamide, dimethyl acetamide and N-methylpyrrolidinone). For this group of solvents, acetonitrile is a relatively poor substitute, especially for reactions involving a strong base.

Solvent selection guide for chromatography

The quick-reference guide for guiding the substitution dichloromethane-methanol in chromatography according to solvent polarity and eluting ability.

ACS Solvent Selection Tool

The American Chemical Society’s Green Chemistry Institute provides an interactive solvent selection tool to select solvents based upon the Principal Component Analysis (PCA) of the solvent’s physical properties. Solvents which are close to each other in the map have similar physical and chemical properties, whereas distant solvents are significantly different. In addition to the PCA scores, physical properties, functional groups, and environmental data are included. See the principles and guidance before using the tool.

TURI Database of Safer Solvents (DOSS)

The Toxics Use Reduction Institute (TURI) provides a solvent database to find solvents that are realistic for your application based on safety, efficiency, and affordability.

• ACS Reagents Guide : Provides a ‘greener’ choice of common chemical reactions.
• Millipore-Sigma DOZN TM Tool : Quantitative Green Chemistry Evaluator to quantify how the chemical synthesis process may impact in resource and energy use and human and environmental hazards. Use this tool to design or modify chemical experiments. Learn more about DOZN TM 0 from the publication or webinar .
• GlaxoSmithKline (GSK) Reagent Guides : reagent guides ranking commonly used reagent for 15 chemical transformations.
• GlaxoSmithKline (GSK) Acid and Base Guides : reagent guides ranking commonly used acids and bases.
• A Guide to Green Chemistry Experiments for Undergraduate Organic Chemistry Labs : Provides list of key publications and websites for greener alternative organic laboratory reactions.
• Higher education curriculum : Open-source green chemistry curriculum for higher education including General Chemistry, Green Chemistry University Curriculum, Organic Chemistry, Toxicology and Virtual Resources.
• Pollution Prevention Options Analysis System (P2OASys) : Assess the potential environmental, worker, and public health impacts of current and alternative processes. Use this tool to compare the current and alternative chemicals on the chemical toxicity, ecological effects, physical properties etc.

Tips: Load the chemicals information from database and compare hazard score summary.

• GreenScreen® for Safer Chemicals : Chemical hazard assessment designed to identify chemicals of high concern and safer alternatives. GreenScreen assessment results can help inform chemical selection decisions at the product design stage, during replacement of hazardous chemicals in existing products, and in procurement.
• Quick Chemical Assessment Tool (QCAT) : Using GreenScreen® as a blueprint, QCAT was developed by the Washington State Department of Ecology to function as a simpler tool for evaluating chemicals/substances to determine their degree of toxicity and assess alternatives.
• Green Lab Supplies and Equipment Guide : List of eco-friendly laboratory equipment and lab consumables.
• Safer Choice-Certified Products and DfE-Certified Disinfectants   : EPA developed the Safer Choice label for cleaners and detergents and the Design for the Environment logo for disinfectants to make it easier for people to find products with ingredients that meet a high standard for human and environmental health.
• ACT Label Database : The ACT label is an eco-nutrition label for laboratory products, including consumables, chemicals, and equipment. By emphasizing accountability, consistency, and transparency (ACT) around manufacturing, energy and water use, packaging, and end-of-life, ACT makes it easy to choose safe, sustainable products.
• Cleaner Solutions Database : Find safe green products for industrial and janitorial applications. Provides information on the effectiveness of different cleaning chemicals and equipment for a variety of surfaces and contaminants.
• Anastas, Paul T.; Warner, John C. (1998). Green Chemistry: Theory and Practice. Oxford [England]; New York: Oxford University Press.
• United States Environmental Protection Agency (EPA) Basics of Green Chemistry
• ACS Green Chemistry
• A Guide to Green Chemistry Experiments for Undergraduate Organic Chemistry Labs from Beyond Benign
• Approaches to Incorporating Green Chemistry and Safety into Laboratory Culture : J. Chem. Educ. , 2021, 98, 84.
• Toxics Use Reduction Institute (TURI) at the University of Massachusetts Lowell
• ACS Green Chemistry: Solvents
• Tools and techniques for solvent selection: green solvent selection guides: Sustainable Chemical Processes , 2016, 4, 7.
• Pfizer solvent selection guide : Green Chemistry , 2008, 10, 31.
• GSK solvent selection guide : Green Chemistry , 2011, 13, 854.
• Sanofi solvent selection guide : Process Res. Dev. , 2013, 17, 12, 1517.
• AstraZeneca solvent selection guide : Process Res. Dev. , 2016, 20, 760.
• Replace dichloromethane in chromatography : Green Chem. , 2012, 14, 3020.
• ACS Division of Organic Chemistry: Green Chemistry
• Green chemistry for chemical synthesis : PNAS , 2008, 105, 13197.
• Green methodologies in organic synthesis: recent developments in our laboratories : Green Chemistry Letters and Reviews , 2013, 6, 189.
• Green Chemistry in Organic Synthesis : Mini-Reviews in Organic Chemistry , 2010, 7, 44.

• Corpus ID: 92956509

Green Organic Chemistry: Strategies, Tools, and Laboratory Experiments

• K. Doxsee , J. Hutchison
• Published 7 May 2003
• Chemistry, Environmental Science

63 Citations

Iodination of vanillin and subsequent suzuki-miyaura coupling: two-step synthetic sequence teaching green chemistry principles.

• Highly Influenced

Statistical Comparison of Results of Redox Titrations Using K-2 CR-2O-7 and KIO-3 in the Undergraduate Analytical Chemistry Lab

Greening wittig reactions: solvent-free synthesis of ethyl trans-cinnamate and trans-3- (9-anthryl)-2-propenoic acid ethyl ester, the cyclohexanol cycle and synthesis of nylon 6,6: green chemistry in the undergraduate organic laboratory, on the applicability of the green chemistry principles to sustainability of organic matter on asteroids, green approach—multicomponent production of boron—containing hantzsch and biginelli esters, a chemical education article- statistical comparison of results of redox titrations using k2cr2o7 and kio3 in the undergraduate analytical chemistry lab, application of the organic on water reactions to prebiotic chemistry, a greener organic chemistry experiment: reduction of citronellal to citronellol using poly(methylhydro)siloxane, green chemistry and the grand challenges of sustainability, related papers.

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Beyond Benign

Green Chemistry Education

Curr Green Chemistry Organic Resource Guide

A guide to green chemistry experiments for undergraduate organic chemistry labs.

Beyond Benign, My Green Lab, and MilliporeSigma have teamed up to develop a comprehensive teaching guide for undergraduate labs featuring Green Chemistry alternatives to traditional organic chemistry experiments and Green Chemistry lab practices.

About the Guide

The organic chemistry laboratory is an opportunity to give students first-hand experience with reactions and techniques central to organic chemistry. Introducing Green Chemistry into the curriculum allows students to continue to learn the fundamentals while also gaining knowledge of Green Chemistry Principles and how they can be used in the lab. For the health of our planet and our people, we believe it is important to train the next generation of chemists to think critically about their chemistry and explore ways to reduce the health and environmental impacts of the molecules they are designing.

That is why Beyond Benign, My Green Lab , and MilliporeSigma have teamed up to develop a comprehensive teaching Guide for undergraduate organic chemistry labs that features Green Chemistry alternatives to traditional organic chemistry experiments. We have recently updated the Guide to include more experiments, an updated introduction, an overview of MilliporeSigma’s DOZN™ 2.0 quantitative Green Chemistry evaluator, and more!

How to download the Guide

You can download the newest version of the guide by completing the form below. Once you complete the form below you will be brought to a download page with multiple resources.

How to request a Greener Solvent Guide magnet

On the download page, sign up to request a Greener Solvent Guide magnet to be shipped to you from Beyond Benign to start making and promoting greener solvent selections in your teaching and research laboratories. These magnets are made from 50% post-industrial recycled material!

To download a copy of the Guide, please complete the form below.

We are requesting this information so that we are aware of who is using this resource. This helps us ensure that future versions of this Guide are beneficial to you. You will only be contacted by us should we update the Guide, have questions about how you are using the Guide, or have a need to communicate relevant information about Green Chemistry experiments for organic chemistry labs. Filling out this form does not add you to our mailing list. If you’d like to be added to our mailing list, sign up for updates at the bottom of the page.

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• Please indicate your role at your organization * Professor Lecturer Graduate Student Undergraduate Student Laboratory Staff Environmental Health and Safety Staff Sustainability Staff Facilities Staff Other
• If you chose "other" above, please specify *
• How did you hear about the guide? * Beyond Benign My Green Lab Webinar Word of Mouth Other
• What are you hoping to learn from the Guide? * Just curious How to implement greener practices in my teaching labs How to implement greener practices in my research Strategies for convincing my colleagues and/or administration to adopt green chemistry Other
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Green organic chemistry : strategies, tools, and laboratory experiments

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Green organic chemistry : strategies, tools, and laboratory experiments

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• Brief Table of Contents. Graphical Abstracts for the Experiments.
• 1. INTRODUCTION.
• 2. IDENTIFICATION AND EVALUATION OF CHEMICAL HAZARDS.
• 3. CHEMICAL EXPOSURE AND ENVIRONMENTAL CONTAMINATION.
• 4. SOURCES OF INFORMATION ABOUT CHEMICAL HAZARDS.
• 5. INTRODUCTION TO GREEN CHEMISTRY.
• 6. ALTERNATIVE SOLVENTS.
• 7. ALTERNATIVE REAGENTS.
• 8. REACTION DESIGN AND EFFICIENCY.
• 9. ALTERNATIVE FEEDSTOCKS AND PRODUCTS.
• 10. THE BIG PICTURE AND GREEN CHEMISTRY METRICS. Laboratory Experiments.
• 11. PREFACE TO THE EXPERIMENTAL SECTION. Experiment
• 1: Solventless Reactions: The Aldol Reaction. Experiment
• 2: Bromination of An Alkene: Preparation of Stilbene Dibromide. Experiment
• 3: A Greener Bromination of Stilbene. Experiment
• 4: Preparation and Distillation of Cyclohexene. Experiment
• 5: Synthesis and Recrystallization of Adipic Acid. Experiment
• 6: Oxidative Coupling of Alkynes: The Glaser-Eglinton-Hay Coupling. Experiment
• 7: Gas-Phase Synthesis, Column Chromatography and Visible Spectroscopy of 5,10,15,20-Tetraphenylporphyrin. Experiment
• 8: Microwave Synthesis of 5,10,15,20-Tetraphenylporphyrin. Experiment
• 9: Metallation of 5,10,15,20-Tetraphenylporphyrin. Experiment
• 10: Measuring Solvent Effects: Kinetics of Hydrolysis of tert-Butyl Chloride. Experiment
• 11: Molecular Mechanics Modeling. Experiment
• 12: Electrophilic Aromatic Iodination. Experiment
• 13: Palladium-Catalyzed Alkyne Coupling/Intramolecular Alkyne Addition: Natural Product Synthesis. Experiment
• 14: Resin-Based Oxidation Chemistry. Experiment
• 15: Carbonyl Chemistry: Thiamine-Mediated Benzoin Condensation of Furfural. Experiment
• 16: Solid-Phase Photochemistry. Experiment
• 17: Applications of Organic Chemistry: Patterning Surfaces With Molecular Films. Experiment
• 18: The Friedel-Crafts Reaction: Acetylation of Ferrocene. Experiment
• 19: Combinatorial Chemistry: Antibiotic Drug Discovery. Appendix A: The Twelve Principles of Green Chemistry.
• (source: Nielsen Book Data)

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Organic Chemistry Laboratory Experiments

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Welcome to the Organic Chemistry Laboratory Experiments repository at OpenBU. We hope that this collection will enable organic chemistry educators to share with other universities valuable experiments performed in the undergraduate teaching laboratory. All lab procedures are available to download and modify, and we encourage the submission of new experiments to the database.

To search the collection: Under the "Browse This Collection" menu on the right-hand side of your screen, you may view the available experiments by author name, title, and subject. Select the desired experiment to view the files available for download. Select either Download or View

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Simple green organic chemistry experiments with the kitchen microwave for high school chemistry classrooms

Microwave systems have been used in organic chemistry since the late 1990s for applications including Microwave-Assisted Organic Synthesis (MAOS). The main advantages of microwave-assisted procedures compared to traditional synthesis methods are the 100- to 1000-fold increase in reaction speeds, higher yields, purer products, and less energy consumption. So far, only a few examples for integrating microwave-induced chemistry into high school chemistry classes have been proposed. This paper presents a set of experiments intended to provide insights into using microwave technology in the context of green, organic chemistry lessons in high school.

Introduction

Microwave technology like Microwave-Assisted Organic Synthesis (MAOS) has been used in industrial organic chemistry since the 1990s ( Lindström et al. 2001 ). MAOS is seen as a contribution to green chemistry ( De la Hoz et al. 2016 ). Microwave technology has become indispensable ( Leadbeater 2010 ), especially in the areas of sustainable organic and polymer chemistry. It has also become very important for pharmaceutical chemistry applications ( Wagner 2006 ). The main advantages of MAOS over traditional synthesis methods are the 100- to 1000-fold increase in reaction rates, higher product yields and purer end products. The quicker reaction speeds are based on the ability of molecules to more readily absorb microwave radiation and convert it into heat. One example in Table 1 given by Mitra et al. (2010) for the synthesis of aspirin, which begins with 18 mL of acetic anhydride and 10 g of salicylic acid, illustrates the potential efficiency of MAOS quite well.

Efficiency of microwave use in the synthesis of aspirin ( Mitra et al. w.y. ).

The efficient use of energy such as that found in MAOS is one of the main principles of green chemistry ( Anastas & Warner 1998 ). Microwave-induced chemistry, however, also tends to save time. In organic chemistry, the spectrum of MAOS applications ranges from organic reactions in solution, organometallic reactions, oxidations, reductions, and polymer syntheses ( Leadbeater 2010 ). Modern microwave-assisted synthesis carried out in industry or the laboratory usually occurs in closed vessels using temperatures above the boiling point of the reaction medium. In a laboratory microwave, integrated magnetic stirrers ensure continuous mixing and sensors allow technicians to control the reaction progress. Several examples using laboratory microwaves have already been published for educational purposes at the undergraduate level (e.g. McGiwan & Leadbeater 2006 ).

One decisive disadvantage of using laboratory microwaves in high schools is their high price. Other problems include the fact that a microwave can only be used by one individual at a time and the fact that a reaction cannot be observed due to the closed reaction vessel. However, the acquisition of laboratory microwaves for use in schools is desirable for the long term, especially in view of the very wide range of applications and the importance of MAOS techniques in modern (green) synthetic chemistry. In the meantime, kitchen microwave ovens can serve as a cheap alternative.

This article describes a set of experiments employing a kitchen microwave. These experiments were selected while developing an organic chemistry curriculum at the senior secondary high school level, which focuses on the different principles of green chemistry ( Linkwitz & Eilks 2020 ). The experiments mostly involved esterification and sought to form either esters, fatty acid methyl esters or polyesters. Other experiments include the decomposition of polylactic acid (PLA) and the extraction of essential oils. All of the above experiments were carried out with the help of a standard household microwave oven. It is recommended that students use a microwave with a split-second timer and a power setting function in watts which is as graduated as possible. We used the OMW3332DM from the German brand OK, which costs about 90€.

When carrying out experiments with kitchen microwaves, certain specific safety issues need to be taken into account ( Mitra et al. 2010 ). Most organic syntheses in laboratory microwave chemistry employ aqueous or other liquid solvents. These solvents tend to be contained in sealed vessels so that reactions can be completed efficiently and quickly. However, pressure measurement is not possible with typical kitchen microwaves. This can lead to unexpected vessel explosions when using sealed vessels. Therefore, school experiments need to take place either at more moderate temperatures or in open or only loosely covered vessels, several of which are described below.

In order to prevent chemicals from coming into contact with students’ skin, eyes, and clothing, participants should wear personal protective equipment such as disposable gloves and eye goggles. All of the carboxylic acids in the experiments can be corrosive in concentrated solution and are irritants in the case of prolonged exposure. All of the alcohols used are flammable. Therefore, they should avoid contact with any ignition sources. 1-octanol may also be absorbed through the skin. Prolonged or repeated contact may dry the skin and cause irritation. The thermal decomposition of Amberlyst 15 may release irritating gases and vapors. Lipase may be harmful if inhaled and may cause eye, skin, and respiratory tract irritation. Potassium hydroxide and sodium hydroxide are highly corrosive and skin contact can cause severely irritability and chemical burns. Glycerine is slightly hazardous in case of ingestion, inhalation, or skin and eye contact. It is also slightly flammable in the presence of heat, open flames, and sparks, as well as oxidizing materials. Ethylene glycol is unlikely to be inhaled at room temperature, but can be toxic if heated, agitate, or sprayed. Polylactic acid may cause eye irritation and may also be harmful if inhaled, absorbed through the skin, or swallowed.

The solutions have to be disposed as organic waste.

Green organic chemistry experiments with a kitchen microwave oven

Experiment 1..

Ester synthesis catalyzed by an acidic ion-exchange resin (Amberlyst 15) (inspired by Reilly et al. 2014 ).

Chemicals: acetic acid, 1-octanol, Amberlyst 15 (A15).

Materials: kitchen microwave, PTFE beaker (100 mL) with top cover ( Figure 1 ).

Time required: approx. 5 min.

Methods: A mixture of 1 mL acetic acid, 2 mL 1-octanol and 0.2 g of A15 are combined in a PTFE beaker (100 mL). The beaker is covered and placed in the household microwave at 400 W for 60 s. The beaker is then removed from the microwave. The presence of 1-octyl acetate can be detected by the moderately intense odor of citrus fruit, which is still strongly masked by acetic acid. The condensed water formed at the cover of the beaker is removed. The reaction is repeated twice under the same parameters (400 W, 60 s). After the third sequence, a pure and intense fruity scent can be confirmed. Other carboxylic acids (e.g. propanoic acid) or alcohols (e.g. 1-butanol) can be used as well. A blank test may be added to see the effect of Amberlyst 15.

PTFE beaker.

Experiment 2.

Ester synthesis catalyzed by lipase (inspired by Yadav & Thorat, 2012 )

Chemicals: acetic acid, 1-octanol, lipase (CalB, Novozym N435)

Materials: kitchen microwave, PTFE beaker (100 mL) with top cover.

Method: A combination of 1 mL acetic acid, 2 mL 1-octanol and a micro-spoon spatula portion of lipase are mixed in a PTFE beaker (100 mL). The beaker is covered and heated in the microwave at 80 W for 60 s. The beaker is then removed from the microwave. 1-octyl acetate can be identified by an intense fruity odor, which is still slightly masked by acetic acid. After a second sequence (80 W, 60 s) of heating, 1-octyl acetate can be clearly identified by a pure fruity odor. If the time interval is shortened to 30 s, a total of three sequences must be run before the pure, intense odor is noticeable. Other carboxylic acids (e.g. propanoic acid) or alcohols (e.g. 1-butanol) can be used as well. A blank test may be added to see the effect of lipase.

Result: An intense fruity sense can be smelled. The carboxylic acid reacts with the alcohol to form a fruit ester (see above).

Experiment 3.

Biodiesel synthesis catalyzed by an acidic ion-exchange resin (Amberlyst 15) or potassium hydroxide (inspired by Mazo et al. 2011 , and Miller & Leadbeater 2009 ).

Chemicals: ethanol, rapeseed oil, Amberlyst 15 (A15), potassium hydroxide, ice.

Materials: kitchen microwave, Erlenmeyer flask, evaporating dish, test tube, spatula, graduated pipette, graduated cylinder.

Method: A total of 1 g of A15 and 5.64 g of rapeseed oil are placed in an Erlenmeyer flask. Then 2.5 mL of ethanol is added. Ethanol is used here instead of methanol because of the higher health risks associated with methanol. The Erlenmeyer flask is covered with a watch glass and some ice is placed on top. Then the Erlenmeyer flask is heated in the microwave at 640 W for 1 min. Afterward the flask is then allowed to cool to room temperature in the microwave. The liquid phase is separated from the Amberlyst 15 and placed in a test tube.

Result of the synthesis of biodiesel in the microwave oven: biodiesel (upper phase of b and c) compared to oil (a).

Experiment 4.

Synthesis of polyesters

Chemicals: glycerine, citric acid, ethylene glycol or castor oil.

Materials: kitchen microwave, watch glass, glass rod, 100 mL beaker.

Method: A total of 1.7 g of glycerine and 7 g of citric acid are combined in the beaker. The beaker is then placed on the edge of the glass turntable in the microwave oven. The mixture is heated at 800 W for 1 min. After waiting for another minute, the microwave is opened and checked to see if the citric acid has completely dissolved. If not, the mixture is heated again until a clear, transparent solution is formed. The solution is poured onto a watch glass.

(source: https://www.researchgate.net/publication/257593270_Instrumental_Physical_Analysis_of_Microwaved_Glycerol_Citrate_Foams/figures?lo=1 ).

Experiment 5.

Decomposition of polylactic acid (PLA).

Chemicals: PLA granulate (crushed), sodium hydroxide, ethanol (50%).

Materials: kitchen microwave, watch glass, 250 mL Erlenmeyer flask, pH-meter.

Method: A total of 5 g of shredded PLA and 5.6 g of sodium hydroxide are put into a 250 mL Erlenmeyer flask. Ethanol is then added until the mixture is covered. The flask is covered with the watch glass. The reaction mixture is heated in a microwave oven at 650 W for no longer than 4 min. It is then allowed to cool for 4 min before repeating the procedure. At 650 W, a total of 4 to 5 cycles are usually required. The mixture is then cooled in an ice bath.

Experiment 6.

Extraction of an essential oil (inspired by Attard et al. 2014 , Chemat et al. 2006 , and Hackleman 2016 )

Chemicals: orange or pomelo peels, ice, water.

Materials: kitchen microwave, grater, beaker (1 L), two beakers (100 mL), plastic funnel with holes, watch glass, volumetric flask (25 mL), pipette.

Time required: approx. 20 min.

Method: The oranges or grapefruits are washed and chopped up in a grater or food processor ( Figure 2 ). The experiment is set up in the microwave as shown in Figure 3 . Heating occurs for 7 min at 600 W. The mixture is allowed to cool for 5–10 min, until the steam has completely condensed in the glass, but not so long that the oil evaporates. The extract is then decanted into the volumetric flask, where the oily phase settles out after a short time. Oranges or pomelos are particularly suitable for this extraction, as you can recognize the oil by its color.

Result: The oily phase settles out after a short time.

Experimental set-up for the extraction of essential oils in the kitchen microwave.

Conclusions

The experiments described above were developed and repeatedly tested while creating a new organic chemistry curriculum at the senior secondary high school level, which focused on the different principles of green chemistry ( Linkwitz & Eilks 2020 ). Our experience with students of age 15–16 shows that the experiments can easily be applied, either as demonstrations or as student activities. Generally, the students were surprised to perform chemical experiments using a kitchen microwave. Reflections after the experiments revealed that the learners had started to see green chemistry as a different approach to doing chemistry. They also recognized that alternative syntheses with the use of microwave radiation can be a part of it.

Author contributions : All authors have accepted responsibility for the entire content of this manuscript and approved its submission.

Research funding : None declared.

Conflict of interest statement : Authors state no conflict of interest.

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© 2022 Michael Linkwitz et al., published by De Gruyter, Berlin/Boston

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A Guide to Green Chemistry Experiments for Undergraduate Organic Chemistry Labs

March 6, 2018 @ 2:00 pm - 3:00 pm est.

Green Chemistry has been widely adopted as a means for reducing hazards and waste in chemistry labs, while maintaining the necessary rigor for teaching fundamental reactions and techniques. In a collaborative partnership between Beyond Benign, My Green Lab, and MilliporeSigma, a new resource guide has been developed for undergraduate organic chemistry teaching labs. This guide provides educators with a set of safer, greener alternative organic chemistry experiments to demonstrate key chemical transformations to undergraduate chemistry students, and indicates quantifiable benefits when greener alternative experiments are implemented, including waste reduction, hazard reduction, and cost savings. Join us on March 6 to learn more about using this new, FREE, customizable guide to educate the next generation of scientists to carry out experiments with sustainability in mind.

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10 Green Chemistry Labs for High School

Chemistry experiments can be pretty daunting.  Some of the basic chemistry experiments students do either in high school or undergraduate studies either use harmful chemicals or produce them.  The point of a green chemistry lab is to reduce and/or eliminate the use of chemicals that are harmful to the environment or to humans. The green chemistry lab activities that I do, could also be classified as kitchen chemistry experiments.  A kitchen chemistry experiment is one that can usually be completed with things you already have in your kitchen. While these green chemistry experiments are great for your kitchen at home, they are also great for your classroom. Here are my top ten green chemistry labs! 

Some reasons you may want to pursue a green chemistry lab:

• you’re not interested exposing yourself or your students to harmful chemicals (not all chemicals are harmful!)
• you’re not interested in the sometimes detailed disposal of harmful chemicals
• you are looking for home school chemistry experiments
• your science budget isn’t what you wished it was, and you are looking for some less expensive alternatives
• you don’t have a full-blown chemistry lab for you and your students to work in (this was my experience my first years of teaching)

If you are in need of a lab rubric, click here to sign up and have an email sent to you!

Oobleck Chemistry Lab Activity

My matter and energy unit comes in the middle of the year as we transition from microchemistry to macrochemistry.  Oobleck is a mixture of cornstarch and water (and food coloring in my classroom). The name “Oobleck” was made famous by the Dr. Seuss book, Bartholomew and the Oobleck.  Essential, oobleck is this goo, (technically a non-Newtonian fluid) that I use to get my students to learn the effect of pressure on phase of matter. When this mixture is allowed to run or is poured (low pressure situations) it will act as if it is a liquid.  As soon as pressure is applied, the oobleck begins to act like a solid. It can be rolled in your hands, but as soon as the rolling action stops, the oobleck will run like liquid through your fingers.

Most students already know that temperature can affect the phase of a sample of matter, but few know about the effects of pressure.  I use this activity to get them to realize that liquids are (mildly) compressible, which leads us to the discussion on how pressure can also be used to change between the phases. 

Atomic Theory Green Chemistry Lab

This Rutherford Model of the Atom lab has been a crowd favorite since I was still working on my Master’s (my pre-teaching days).  You and your students model Rutherford’s Gold Foil Experiment. Essentially you have students throw ping-pong balls which represent alpha particles, toward your Rutherford model.  The model is constructed from a hula-hoop, and a ball dangling in the center which represents the nucleus. Depending on how advanced your curriculum or standards are, you can talk about the nucleus to atom size ratio and the validity of models in science. You can read more about that experiment here.

Spectral Lines Chemistry Lab

Now depending on how you look at this, this may or may not be a green chemistry lab. For me, it is. This lab is not something I would have been able to do in my lab-less situation during my early years of teaching, so I understand the argument – trust me. This lab technically does not produce chemicals that are harmful to you or the environment, and as long as you have the proper equipment it’s super simple. It’s essentially a point and shoot. Turn off the lights, draw the shades and let the kids read their hand-held spectroscopes and determine the identify of the gas in the tube. Most of these tubes get pretty toasty, so be careful!

Factors that Affect Solubility Lab

This lab is only for the solubility of solids and the factors that help them dissolve. Here, students are working with sugar and water and they test three different variables for solubility of solids: surface area, agitation and temperature. My students go crazy for this lab simply because so few of them have ever seen a sugar cube in real life. I mean who even uses them anymore? I sometimes have a hard time finding them in the store, but I can usually find them on the very bottom shelf at my grocery store. You can read more about this specific lab here.

Effects of Intermolecular Forces

Intermolecular forces are really tough to demonstrate, but their effects are super easy to see! Surface tension is one of my favorite effects of intermolecular forces, simply due to the relation to real life. In this lab , you’d take a penny (simply because they are smaller, so data is quicker to collect) and count the number of drops of different substances that fit on its surface. You can do this plain water, salt water and soapy water, or you can use different oils, like baby oil or vegetable oil. Just make sure to clean the penny in between each trial.

Intro to Stoichiometry Lab

This lab is for basic gram and mole conversions. Students find the mass of a few basic things in your classroom and convert those masses to moles. This lab gets students prepared for some of the bigger “math of chemistry” and stoichiometry skills that will be coming their way. My favorite part of this lab is when students write their names on the board and find out how many moles of chalk it takes to do it. Many of them write the sweetest messages, or draw silly pictures.

Like Dissolves Like Lab Activity

Depending on how you take this lab , this could be a green chemistry lab. In this lab, students mix different solutions with water to check its molecular polarity. I’ve made homemade Aqua Sand that I mix into the lab to make it super engaging for my students. This requires sand to be sprayed with some waterproofing camping spray – so maybe this isn’t entirely green. If you ditch the Aqua Sand , it totally is though! If you’re not happy with this being a part of the list, I’ve added a bonus green chemistry lab at the end of this post for you! You can read more about this specific activity and the hydrophobic sand, check out this blog post.

Acid-Base Kitchen Chemistry Lab

Did you know that cabbage juice is an acid-base indicator?  So cool, right?! Well this is a great introduction lab for standards and stock solutions.  My students boil some red cabbage to get the juice. But you can do this at home the night before. Or even just let the cabbage soak in water for a bit.  The darker the purple color the better! Then in a spot plate, put a few drops of solutions with known pH values and create an indicator color chart.

In order to keep this “authentically green chemistry” then you would use regular household items, like lemon juice, and soaps. There are plenty of household items to test! Maybe, even have your students bring in a sample of something they are interested in testing! You can also give the students a few unknowns to test, to compare to the knowns.  If you wanted to be “super sciencey” with this, you can then move the unknown solutions into a titration to be totally sure of the pH value.

Kinetics Green Chemistry Lab

This lab requires a trip to the beauty supply store.  You’ll need to get some liquid developer , which is really a hydrogen peroxide solution. This is stronger than hydrogen peroxide from the drugstore for cuts).  Mix this with some liquid dish soap and swirl it around. I let my students add food coloring to make this a bit more interesting. You will need to add this solution to the “reaction vessel”  which for me is an Erlenmeyer. I like to leave these directly on my lab bench and squeegee the mess into the sink. If you don’t have that option, I suggest placing the Erlenmeyer in a disposable aluminum baking pan.

In a beaker, mix some warm water with some instant yeast.  If you don’t have instant yeast, give this solution a few minutes to “activate.” Five or ten minutes will do. The yeast is your catalyst for ripping the oxygen off the peroxide. Pour the yeast mixture into the reaction vessel and BOOM! you have kinetics! This same reaction would not happen without the yeast (you can of course have your students try it). This leads to a great discussion on activation energy and the use of catalysts.  This lab is one of my favorites because it reminds me of when my childhood friend Emily and I would mix vinegar and baking soda on the curb and let it run down the street. What can I say, I’ve been a science nerd forever.

Organic Chemistry Green Chemistry Lab

If you have a child aged 5-18 during the years 2014-2017 you lived through the “Slime Era” of the internet.  Fortunately for you, I started my teaching career during this time and I used that to my advantage! Technically, making slime out of glue is a polymerization, meaning when the kids make the slime, they are actually completing a chemical reaction !  There are a million recipes out there, but we use a simple, cheap and easy recipe.

You’ll need some glue , and a box of Borax and some disposable or preferably reusable bowls and spoons. That box of Borax will last forever, trust me. Mix equal amounts of glue and water in a bowl.  Gently mix (whisking motions) until thoroughly combined. Add in food coloring and glitter if desired. I make a “master solution” of the polymerizer. I take around 2 tablespoons of Borax per liter of water and distribute it to the kids in cups. They then mix the solution with their glue until they get a polymer.  When you think the mixture needs “just a little bit more” solution, it is time to massage the slime by hand. If the slime is “over-polymerized” you can add some water until it softens up. My students get to bring their slime home in sandwich bags. It is such a fun time!

Bonus: Solutions Green Chemistry Lab

The holy grail of chemistry labs – making ice cream by the science of freezing point depression.  I have my students bring in toppings, salt and bowls. I bring the milk. We have an ice machine in the school, so I bring a cooler and have a few kids go pick it up and haul the cooler to my room. Here’s the steps:

• Fill a gallon bag about halfway with ice and pour a generous amount of rock/coarse/Kosher salt.
• Inside a sandwich sized bag , add 1 cup of milk, half a cup of sugar. Or less – I have the students stick their finger in the bag for a taste test). And ¼ teaspoon of vanilla extract.  For chocolate icecream I have the kids do 1 cup of milk with ⅓ to ½ a cup of Nesquik for the flavor. (Cocoa powder is too bitter for most kids). 
• Put the sandwich bag inside the gallon bag, and maneuver so that the sandwich bag is surrounded. 
• Shake until milk is firm.

Obviously this only works with the salt in the bag because the salt, drops the freezing point of the ice. Viola! You have ice cream and a Colligative Properties Lab Activity ! You can read more about my ice cream lab here !

I hope that these green chemistry labs help you to make environmentally conscious changes in your classroom that both you and your students will love and remember for years to come! You can read more about how my students write lab reports here .

*This post contains affiliate links, meaning that if you make a purchase through the link I make a small commission. Though this does not affect the price of the item for the customer.

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Comprehensive Organic Chemistry Experiments for the Laboratory Classroom

This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment.

Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.

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Comprehensive Organic Chemistry Experiments for the Laboratory Classroom, The Royal Society of Chemistry, 2016.

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• Front Matter
• 1.1. Separation, Purification and Identification of the Components of a Mixture p1-5 By Abel J. S. C. Vieira ; Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elvira M. S. M. Gaspar Elvira M. S. M. Gaspar Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.1. Separation, Purification and Identification of the Components of a Mixture in another window
• 1.2. Isolation of (+)-Limonene from Orange Oil p6-8 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.2. Isolation of (+)-Limonene from Orange Oil in another window
• 1.3. Isolation of Plant Pigments from Green and Red Leaves p9-13 By Alice M. Dias ; Alice M. Dias Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria La S. Ferreira Maria La S. Ferreira Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.3. Isolation of Plant Pigments from Green and Red Leaves in another window
• 1.4. Extraction of Usnic Acid from Lichen p14-17 By Dietmar K. Kennepohl Dietmar K. Kennepohl Athabasca University   1 University Drive   Athabasca   Alberta   T9S 3A3   Canada   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.4. Extraction of Usnic Acid from Lichen in another window
• 1.5. Thin-Layer Chromatography of Plants Pigments p18-22 By Ana Margarida Madureira ; Ana Margarida Madureira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.5. Thin-Layer Chromatography of Plants Pigments in another window
• 1.6. Isolation of Cinnamaldehyde from Cinnamon p23-25 By Raquel F. M. Frade ; Raquel F. M. Frade iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dulce Simão ; Dulce Simão Department of Chemical Engineering, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.6. Isolation of Cinnamaldehyde from Cinnamon in another window
• 1.7. Isolation and Structural Identification of Piperine, the Major Alkaloid of Black Pepper p26-29 By Andreia Mónico ; Andreia Mónico iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Angela Paterna ; Angela Paterna iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mariana A. Reis ; Mariana A. Reis iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ricardo Ferreira ; Ricardo Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Noélia Duarte ; Noélia Duarte iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana M. Madureira ; Ana M. Madureira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.7. Isolation and Structural Identification of Piperine, the Major Alkaloid of Black Pepper in another window
• 1.8. Caffeine Extraction from Tea and Coffee p30-34 By Ana Margarida Madureira ; Ana Margarida Madureira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Abel J. S. C. Vieira ; Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa, Campus de Caparica   2829-516 Caparica, Caparica   Portugal Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.8. Caffeine Extraction from Tea and Coffee in another window
• 1.9. Isolation of the Alkaloid Lupanine from Lupinus albus Seeds p35-37 By Ana M. Lourenço ; Ana M. Lourenço REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luísa Maria Ferreira Luísa Maria Ferreira REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.9. Isolation of the Alkaloid Lupanine from <em>Lupinus albus</em> Seeds in another window
• 1.10. Isolation and Purification of Atropine, a Tropane Alkaloid Obtained from Atropa belladonna L. (Solanaceae) p38-42 By Gustavo da Silva Gustavo da Silva Department of Pharmacological Sciences, Research Institute for Medicines and Pharmaceutical Sciences (iMed.ULisboa), Faculty of Pharmacy – University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.10. Isolation and Purification of Atropine, a Tropane Alkaloid Obtained from <em>Atropa belladonna</em> L. (Solanaceae) in another window
• 1.11. Isolation and Purification of Carnosol from Salvia officinalis † p43-45 By Filipe Pereira ; Filipe Pereira Universidade Lusófona Research Center for Biosciences & Health Technologies (CBIOS)   Campo Grande   376   1749-024 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Patrícia Rijo Patrícia Rijo Universidade Lusófona Research Center for Biosciences & Health Technologies (CBIOS)   Campo Grande   376   1749-024 Lisboa   Portugal Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.11. Isolation and Purification of Carnosol from <em>Salvia officinalis</em>^{<a href="javascript:;" reveal-id="BK9781849739634-00043-fn1" data-open="BK9781849739634-00043-fn1" class="link link-ref link-reveal xref-fn js-xref-fn split-view-modal">†</a>} in another window
• 1.12. Analysis of Racemic and ( S )-Ibuprofen p46-50 By C. Fernandes ; C. Fernandes Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar H. Cidade ; H. Cidade Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar S. Cravo ; S. Cravo Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar E. Sousa ; E. Sousa Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Pinto M. Pinto Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.12. Analysis of Racemic and (<em>S</em>)-Ibuprofen in another window
• 1.13. Determining Partition Coefficients of Sulfonamides by Reversed-Phase Chromatography p51-55 By E. Sousa ; E. Sousa Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar S. Cravo ; S. Cravo Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar C. Fernandes ; C. Fernandes Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Pinto M. Pinto Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto   Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.13. Determining Partition Coefficients of Sulfonamides by Reversed-Phase Chromatography in another window
• 2.1.1. A S N 1 Reaction: Synthesis of tert -Butyl Chloride p56-60 By Emília Valente ; Emília Valente Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Luís Constantino Luís Constantino Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.1. A S_N1 Reaction: Synthesis of <em>tert</em>-Butyl Chloride in another window
• 2.1.2. Optimizing the Reaction Conditions for the Synthesis of tert -Pentyl Chloride p61-63 By Jane Brock Greco Jane Brock Greco Department of Chemistry, Johns Hopkins University   3400 N. Charles St. Baltimore   MD 21218   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.2. Optimizing the Reaction Conditions for the Synthesis of <em>tert</em>-Pentyl Chloride in another window
• 2.1.3. Kinetics of a S N 1 Reaction p64-67 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.3. Kinetics of a S_N1 Reaction in another window
• 2.1.4. Counterion Effects in the Nucleophilic Substitution Reaction of the Acetate Ion with Alkyl Bromides in the Synthesis of Esters p68-71 By Ingrid Montes ; Ingrid Montes Department of Chemistry, University of Puerto Rico-Río Piedras Campus   PO Box 23346   San Juan   PR 00931-3346   Puerto Rico   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Elizabeth Valentín ; M. Elizabeth Valentín Department of Chemistry, University of Puerto Rico-Río Piedras Campus   PO Box 23346   San Juan   PR 00931-3346   Puerto Rico   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Waldemar Adam Waldemar Adam Department of Chemistry, University of Puerto Rico-Río Piedras Campus   PO Box 23346   San Juan   PR 00931-3346   Puerto Rico   USA   [email protected] Institute of Organic Chemistry, University of Wuerzburg   Am Hubland   D-97094 Wuerzburg   Germany Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.4. Counterion Effects in the Nucleophilic Substitution Reaction of the Acetate Ion with Alkyl Bromides in the Synthesis of Esters in another window
• 2.1.5. N -Alkylation of Pyrazole: Reaction in an Ionic Liquid p72-75 By Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Geórgia C. Zimmer ; Geórgia C. Zimmer Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilherme C. Paveglio ; Guilherme C. Paveglio Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Helio G. Bonacorso Helio G. Bonacorso Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.5. <em>N</em>-Alkylation of Pyrazole: Reaction in an Ionic Liquid in another window
• 2.1.6. Conversion of Alcohols into Alkyl Chlorides Using Cyanuric Chloride p76-79 By Eliana Martins ; Eliana Martins Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina A. B. Rodrigues ; Catarina A. B. Rodrigues Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.6. Conversion of Alcohols into Alkyl Chlorides Using Cyanuric Chloride in another window
• 2.1.7. Synthesis of Phenacetin p80-83 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.7. Synthesis of Phenacetin in another window
• 2.1.8. One-Step Synthesis of 4(3 H )-Quinazolinones: An Important Heterocyclic Scaffold in Medicinal Chemistry p84-86 By André Dias ; André Dias Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira ; Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição Ana S. Ressurreição Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.8. One-Step Synthesis of 4(3<em>H</em>)-Quinazolinones: An Important Heterocyclic Scaffold in Medicinal Chemistry in another window
• 2.1.9. Controlled Monoalkylation of the Structurally Rigid Bicyclic System Isomannide p87-91 By M. Manuela ; M. Manuela REQUIMTE, Chemistry Department, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   2827-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar A. Pereira A. Pereira REQUIMTE, Chemistry Department, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   2827-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.9. Controlled Monoalkylation of the Structurally Rigid Bicyclic System Isomannide in another window
• 2.1.10. Regioselective N -alkylation of Adenine by Nucleophilic Substitution p92-94 By Ana I. Vicente ; Ana I. Vicente iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.10. Regioselective <em>N</em>-alkylation of Adenine by Nucleophilic Substitution in another window
• 2.1.11. Gabriel Synthesis of n -Octylamine Under Phase-Transfer Catalysis: The First Step p95-98 By Renata Riva ; Renata Riva Search for other works by this author on: This Site PubMed Google Scholar Luca Banfi Luca Banfi Dipartimento di Chimica e Chimica Industriale   Via Dodecaneso 31   16146 Genova   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.11. Gabriel Synthesis of <em>n</em>-Octylamine Under Phase-Transfer Catalysis: The First Step in another window
• 2.1.12. Preparation of Diethyl 2,3- O -isopropylidene- l -tartrate p99-102 By Naylil M. R. Capreti ; Naylil M. R. Capreti Institute of Chemistry, State University of Campinas (Unicamp)   C.P. 6154   13083-970   Campinas   SP   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Igor D. Jurberg Igor D. Jurberg Institute of Chemistry, State University of Campinas (Unicamp)   C.P. 6154   13083-970   Campinas   SP   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.12. Preparation of Diethyl 2,3-<em>O</em>-isopropylidene-<span class="small-caps">l</span>-tartrate in another window
• 2.1.13. Redox-Neutral Synthesis of a Cyclic N , O -Acetal from Salicylaldehyde and 1,2,3,4-Tetrahydroisoquinoline p103-106 By Claire L. Jarvis ; Claire L. Jarvis Rutgers, the State University of New Jersey, Department of Chemistry and Chemical Biology, Rutgers University   610 Taylor Road   Piscataway   NJ 08854-8087   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Daniel Seidel Daniel Seidel Rutgers, the State University of New Jersey, Department of Chemistry and Chemical Biology, Rutgers University   610 Taylor Road   Piscataway   NJ 08854-8087   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.13. Redox-Neutral Synthesis of a Cyclic <em>N</em>,<em>O</em>-Acetal from Salicylaldehyde and 1,2,3,4-Tetrahydroisoquinoline in another window
• 2.2.1. Selective C -acylation of 3-Methyl-1-phenyl-pyrazol-5-one p107-111 By Vanya B. Kurteva ; Vanya B. Kurteva Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences   Acad. G. Bonchev str., bl. 9   1113   Sofia   Bulgaria   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Lubomir A. Lubenov ; Lubomir A. Lubenov Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences   Acad. G. Bonchev str., bl. 9   1113   Sofia   Bulgaria   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria A. Petrova Maria A. Petrova University of Chemical Technology and Metallurgy, Department of General and Inorganic Chemistry   8 Kliment Ohridski blvd.   1756 Sofia   Bulgaria Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.1. Selective <em>C</em>-acylation of 3-Methyl-1-phenyl-pyrazol-5-one in another window
• 2.2.2. Organocatalytic Asymmetric α-Arylation of Aldehydes p112-116 By Mette Overgaard ; Mette Overgaard Department of Chemistry, Aarhus University   DK-8000 Aarhus C   Denmark   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pernille H. Poulsen ; Pernille H. Poulsen Department of Chemistry, Aarhus University   DK-8000 Aarhus C   Denmark   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Karl Anker Jørgensen Karl Anker Jørgensen Department of Chemistry, Aarhus University   DK-8000 Aarhus C   Denmark   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.2. Organocatalytic Asymmetric α-Arylation of Aldehydes in another window
• 2.2.3. Matteson Homologation of Pinacol Boronic Ester: An Efficient Method Using the Boronate Complexes p117-119 By Sébastien Balieu ; Sébastien Balieu Université de Rouen, IRCOF   1 Rue Tesnières - 76130 Mont Saint Aignan   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Asmaa Bouyahya ; Asmaa Bouyahya Université de Rouen, IRCOF   1 Rue Tesnières - 76130 Mont Saint Aignan   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jean-Philippe Bouillon Jean-Philippe Bouillon Université de Rouen, IRCOF   1 Rue Tesnières - 76130 Mont Saint Aignan   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.3. Matteson Homologation of Pinacol Boronic Ester: An Efficient Method Using the Boronate Complexes in another window
• 2.2.4. A Practical Organocatalytic Alkylation Reaction with Benzodithiolylium Tetrafluoroborate p120-124 By Pier Giorgio Cozzi ; Pier Giorgio Cozzi Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician”   Via Selmi 2   40126 Bologna   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marco Bandini ; Marco Bandini Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician”   Via Selmi 2   40126 Bologna   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrea Gualandi ; Andrea Gualandi Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician”   Via Selmi 2   40126 Bologna   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luca Mengozzi Luca Mengozzi Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician”   Via Selmi 2   40126 Bologna   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.4. A Practical Organocatalytic Alkylation Reaction with Benzodithiolylium Tetrafluoroborate in another window
• 2.2.5. Oxazolidinone Mediated Enantioselective Allylation p125-128 By Jonathan D. Sellars ; Jonathan D. Sellars Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar AnnMarie C. O’Donoghue ; AnnMarie C. O’Donoghue Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ian R. Baxendale ; Ian R. Baxendale Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar John M. Sanderson ; John M. Sanderson Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elizabeth J. Grayson Elizabeth J. Grayson Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.5. Oxazolidinone Mediated Enantioselective Allylation in another window
• 3.1.1. Synthesis of Paracetamol by Acetylation p129-132 By Catarina Dias ; Catarina Dias Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Emília Valente ; Emília Valente Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Luís Constantino Luís Constantino Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.1. Synthesis of Paracetamol by Acetylation in another window
• 3.1.2. Synthesis and Characterization of N , N ′-Dicyclohexyl- N , N ′-dimethyl-propan-1,3-diamide p133-135 By Ana Paula Paiva ; Ana Paula Paiva Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   Rua Ernesto de Vasconcelos, C8, Campo Grande   1749-016 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Osvaldo Ortet Osvaldo Ortet Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   Rua Ernesto de Vasconcelos, C8, Campo Grande   1749-016 Lisbon   Portugal   [email protected] Departamento de Ciência e Tecnologia, Universidade de Cabo Verde   379C   Praia   Santiago Island   Cape Verde Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.2. Synthesis and Characterization of <em>N</em>,<em>N</em>′-Dicyclohexyl-<em>N</em>,<em>N</em>′-dimethyl-propan-1,3-diamide in another window
• 3.1.3. Synthesis and Characterisation of an Ester from 4-Nitrobenzoyl Chloride p136-138 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Matt L. Clarke ; Matt L. Clarke School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Leanne Harris ; Leanne Harris School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrew. J. Miller Andrew. J. Miller School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.3. Synthesis and Characterisation of an Ester from 4-Nitrobenzoyl Chloride in another window
• 3.1.4. Green Esterification: The Synthesis of Aromas in the Presence of an Acid Resin p139-141 By José E. Castanheiro ; José E. Castanheiro Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho, no. 59   7000-671 Évora   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar António P. S. Teixeira ; António P. S. Teixeira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho, no. 59   7000-671 Évora   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar António M. D. R. L. Pereira António M. D. R. L. Pereira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho, no. 59   7000-671 Évora   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.4. Green Esterification: The Synthesis of Aromas in the Presence of an Acid Resin in another window
• 3.1.5. Acetylation of Cholesterol and Purification by Column Chromatography p142-146 By Emília Valente ; Emília Valente Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Luís Constantino Luís Constantino Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.5. Acetylation of Cholesterol and Purification by Column Chromatography in another window
• 3.1.6. Synthesis of Hippuric Acid: An Example of Amide Bond Formation p147-150 By Ana S. Ressurreição ; Ana S. Ressurreição Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria de Jesus Perry ; Maria de Jesus Perry Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Paula Francisco ; Ana Paula Francisco Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes Francisca Lopes Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.6. Synthesis of Hippuric Acid: An Example of Amide Bond Formation in another window
• 3.1.7. Preparation of a Sulfathiazole Prodrug via N -acylation with Succinic Anhydride p151-153 By Pedro M. P. Gois ; Pedro M. P. Gois Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes ; Francisca Lopes Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandre F. Trindade Alexandre F. Trindade Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.7. Preparation of a Sulfathiazole Prodrug <em>via N</em>-acylation with Succinic Anhydride in another window
• 3.1.8. Determination of the Absolute Configuration of Enantioenriched Secondary Alcohols via Thin-Layer Chromatography p154-158 By Alexander J. Wagner ; Alexander J. Wagner Department of Chemistry, University of California–Irvine   1102 Natural Sciences II   Irvine   CA 92697   USA   [email protected]   [email protected]   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Shawn M. Miller ; Shawn M. Miller Department of Chemistry, University of California–Irvine   1102 Natural Sciences II   Irvine   CA 92697   USA   [email protected]   [email protected]   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Scott D. Rychnovsky ; Scott D. Rychnovsky Department of Chemistry, University of California–Irvine   1102 Natural Sciences II   Irvine   CA 92697   USA   [email protected]   [email protected]   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renée D. Link Renée D. Link Department of Chemistry, University of California–Irvine   1102 Natural Sciences II   Irvine   CA 92697   USA   [email protected]   [email protected]   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.8. Determination of the Absolute Configuration of Enantioenriched Secondary Alcohols <em>via</em> Thin-Layer Chromatography in another window
• 3.1.9. Anhydride Aminolysis: Synthesis of N -arylmaleamic Acids p159-161 By Artur M. S. Silva ; Artur M. S. Silva Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.9. Anhydride Aminolysis: Synthesis of <em>N</em>-arylmaleamic Acids in another window
• 3.1.10. Synthesis of N -arylmaleimides p162-164 By Artur M. S. Silva ; Artur M. S. Silva Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.10. Synthesis of <em>N</em>-arylmaleimides in another window
• 3.1.11. Synthesis and Characterization of N -Cyclohexyl- N- methyloctanamide p165-168 By Ana Paula Paiva ; Ana Paula Paiva Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Osvaldo Ortet Osvaldo Ortet Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   Lisboa   Portugal   [email protected] Departamento de Ciência e Tecnologia, Universidade de Cabo Verde   Praia   Cape Verde Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.11. Synthesis and Characterization of <em>N</em>-Cyclohexyl-<em>N-</em>methyloctanamide in another window
• 3.1.12. Effect of a Catalyst in the Acylation of Alcohols with Acetic Anhydride: Manipulation of a Natural Aroma p169-171 By Mónica S. Estevão ; Mónica S. Estevão iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.12. Effect of a Catalyst in the Acylation of Alcohols with Acetic Anhydride: Manipulation of a Natural Aroma in another window
• 3.1.13. Synthesis of 4,5-Dichloro-1,2-dicyanobenzene p172-174 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.13. Synthesis of 4,5-Dichloro-1,2-dicyanobenzene in another window
• 3.1.14. Synthesis of N-tert -Butyloxycarbonyl-3-nitro- l -tyrosine Methyl Ester p175-177 By Susana P. G. Costa ; Susana P. G. Costa University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Manuela M. Raposo ; M. Manuela M. Raposo University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cátia I. C. Esteves ; Cátia I. C. Esteves University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar R. Cristina M. Ferreira R. Cristina M. Ferreira University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.14. Synthesis of <em>N-tert</em>-Butyloxycarbonyl-3-nitro-<span class="small-caps">l</span>-tyrosine Methyl Ester in another window
• 3.1.15. Michael Addition Reaction Followed by Elimination Under Solvent-Free Conditions p178-181 By Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilherme C. Paveglio ; Guilherme C. Paveglio Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Geórgia C. Zimmer ; Geórgia C. Zimmer Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nilo Zanatta Nilo Zanatta Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.15. Michael Addition Reaction Followed by Elimination Under Solvent-Free Conditions in another window
• 3.1.16. Synthesis of a γ-Keto-amide Derived from Thiophene Using a Carboxyl Ester as Precursor p182-187 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.16. Synthesis of a γ-Keto-amide Derived from Thiophene Using a Carboxyl Ester as Precursor in another window
• 3.1.17. Cyclic Acetals for Regioselective Protection in Carbohydrate Synthesis: A Comparative Experiment p188-193 By Ana M. Matos ; Ana M. Matos Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   C8, Piso 5, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rafael Nunes ; Rafael Nunes Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   C8, Piso 5, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   C8, Piso 5, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Amélia P. Rauter Amélia P. Rauter Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   C8, Piso 5, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.17. Cyclic Acetals for Regioselective Protection in Carbohydrate Synthesis: A Comparative Experiment in another window
• 3.1.18. Direct Diastereoselective Synthesis of the Tetrahydro-thiazolo[2,3- b ]isoindole Tricyclic Ring System p194-197 By Maria I. L. Soares ; Maria I. L. Soares Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Lúcia Cardoso ; Ana Lúcia Cardoso Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana M. M. Lopes ; Susana M. M. Lopes Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Teresa M. V. D. Pinho e Melo Teresa M. V. D. Pinho e Melo Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.18. Direct Diastereoselective Synthesis of the Tetrahydro-thiazolo[2,3-<em>b</em>]isoindole Tricyclic Ring System in another window
• 3.1.19. Asymmetric Cyclocondensation Reaction Induced by Chiral Aminoalcohol p198-201 By Jorge Dourado ; Jorge Dourado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria Pérez ; Maria Pérez Laboratory of Organic Chemistry, Faculty of Pharmacy and Institute of Biomedicine (IBUB), University of Barcelona   Av. Joan XXIII, s/n   08028 Barcelona   Spain Search for other works by this author on: This Site PubMed Google Scholar Rosa Griera ; Rosa Griera Laboratory of Organic Chemistry, Faculty of Pharmacy and Institute of Biomedicine (IBUB), University of Barcelona   Av. Joan XXIII, s/n   08028 Barcelona   Spain Search for other works by this author on: This Site PubMed Google Scholar Maria M. M. Santos Maria M. M. Santos Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.19. Asymmetric Cyclocondensation Reaction Induced by Chiral Aminoalcohol in another window
• 3.1.20. Synthesis and Characterization of Biodiesel Propyl Esters to Determine the Fatty Acid Content of Unknown Plant Oils p202-205 By Heidi R. Vollmer-Snarr ; Heidi R. Vollmer-Snarr Department of Chemistry, Stanford University   S.G. Mudd Bldg., 333 Campus Drive   Stanford   CA 94305-4401   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Patrick A. Fracisco ; Patrick A. Fracisco Department of Chemistry, Stanford University   S.G. Mudd Bldg., 333 Campus Drive   Stanford   CA 94305-4401   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Naiian Saephanh Naiian Saephanh Department of Chemistry, Stanford University   S.G. Mudd Bldg., 333 Campus Drive   Stanford   CA 94305-4401   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.20. Synthesis and Characterization of Biodiesel Propyl Esters to Determine the Fatty Acid Content of Unknown Plant Oils in another window
• 3.2.1. Synthesis of 7-Methoxy-4-oxo- N -phenyl-4 H -chromene-2-carboxamide p206-211 By Joana Reis ; Joana Reis Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Gaspar ; Alexandra Gaspar Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Cagide ; Fernando Cagide Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges Fernanda Borges Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.1. Synthesis of 7-Methoxy-4-oxo-<em>N</em>-phenyl-4<em>H</em>-chromene-2-carboxamide in another window
• 3.2.2. Synthesis of 2,3-Diphenylindenone p212-215 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.2. Synthesis of 2,3-Diphenylindenone in another window
• 3.2.3. Synthesis of Dimedone p216-218 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.3. Synthesis of Dimedone in another window
• 3.2.4. Acylation Reaction of Enol Ether Using an Ionic Liquid p219-222 By Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Geórgia C. Zimmer ; Geórgia C. Zimmer Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nilo Zanatta Nilo Zanatta Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.4. Acylation Reaction of Enol Ether Using an Ionic Liquid in another window
• 4.1.1.1. Bromination of Cinnamic Acid p223-225 By Paulo Coelho ; Paulo Coelho Centro de, Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de, Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.1. Bromination of Cinnamic Acid in another window
• 4.1.1.2. Preparation of Meso -1,2-Dibromo-1,2-diphenylethane p226-228 By Abel J. S. C. Vieira Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.2. Preparation of <em>Meso</em>-1,2-Dibromo-1,2-diphenylethane in another window
• 4.1.1.3. Bromination of ( E )-chalcones [( E )-1,3-Diarylprop-2-en-1-ones] p229-230 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.3. Bromination of (<em>E</em>)-chalcones [(<em>E</em>)-1,3-Diarylprop-2-en-1-ones] in another window
• 4.1.1.4. Preparation of trans -2-Bromocyclohexanol from Cyclohexanol p231-233 By Matheus P. Freitas Matheus P. Freitas Department of Chemistry, Federal University of Lavras   37200-000   Lavras   MG   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.4. Preparation of <em>trans</em>-2-Bromocyclohexanol from Cyclohexanol in another window
• 4.1.1.5. Synthesis of trans -Cyclohexane-1,2-diol p234-236 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.5. Synthesis of <em>trans</em>-Cyclohexane-1,2-diol in another window
• 4.1.1.6. Synthesis of Isobutylene and Its Use in Esterification Reactions p237-240 By Paula C. Castilho ; Paula C. Castilho Centro de Química da, Madeira, Universidade da Madeira, Campus Universitário da Penteada   Piso 00   9020-105   Funchal   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro Ideia ; Pedro Ideia Centro de Química da, Madeira, Universidade da Madeira, Campus Universitário da Penteada   Piso 00   9020-105   Funchal   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rúben Gonçalves Rúben Gonçalves Centro de Química da, Madeira, Universidade da Madeira, Campus Universitário da Penteada   Piso 00   9020-105   Funchal   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.6. Synthesis of Isobutylene and Its Use in Esterification Reactions in another window
• 4.2.3.8. Synthesis of a Long-Wavelength Absorbing Squaraine Dye p396-398 By Paulo F. Santos ; Paulo F. Santos Departamento de Química and Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Vânia C. Graça Vânia C. Graça Departamento de Química and Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.8. Synthesis of a Long-Wavelength Absorbing Squaraine Dye in another window
• 4.2.3.9. Synthesis of π-Conjugated Systems Using Formylchromone as Building Block p399-402 By Carlos Fernandes ; Carlos Fernandes CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina Oliveira ; Catarina Oliveira CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges ; Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Gaspar Alexandra Gaspar CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.9. Synthesis of π-Conjugated Systems Using Formylchromone as Building Block in another window
• 4.2.3.10. A Multi-Step Synthesis of Imidazolin-5-ones p403-407 By Gurunath Ramanathan ; Gurunath Ramanathan Indian Institute of Technology Kanpur   Kanpur 208016   India   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ashish Singh Ashish Singh Indian Institute of Technology Kanpur   Kanpur 208016   India   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.10. A Multi-Step Synthesis of Imidazolin-5-ones in another window
• 4.2.3.11. Baylis–Hillman Reaction Between 4-Nitrobenzaldehyde and Ethyl Acrylate p408-410 By Alexandre F. Trindade ; Alexandre F. Trindade Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar João Ravasco ; João Ravasco Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.11. Baylis–Hillman Reaction Between 4-Nitrobenzaldehyde and Ethyl Acrylate in another window
• 4.1.1.7. Hydroxyl Group Protection via Tetrahydropyranyl Ether Formation p241-243 By Ana I. B. Meirinhos ; Ana I. B. Meirinhos iMed.ULisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Filipa Siopa ; Filipa Siopa iMed.ULisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.7. Hydroxyl Group Protection <em>via</em> Tetrahydropyranyl Ether Formation in another window
• 4.1.1.8. Synthesis of (−)-Carvone from (+)-Limonene p244-246 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.8. Synthesis of (−)-Carvone from (+)-Limonene in another window
• 4.2.3.12. Synthesis of Ethyl Mandelate Through a Rhodium-Catalysed Arylation Reaction with Ethyl Glyoxylate and Phenylboronic Acid p411-414 By Carolina S. Marques ; Carolina S. Marques University of Évora, Chemistry Department, School of Science and Technology, Centro de Química de Évora, Institute for Research and Advanced Training   Rua Romão Ramalho, 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anthony J. Burke Anthony J. Burke University of Évora, Chemistry Department, School of Science and Technology, Centro de Química de Évora, Institute for Research and Advanced Training   Rua Romão Ramalho, 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.12. Synthesis of Ethyl Mandelate Through a Rhodium-Catalysed Arylation Reaction with Ethyl Glyoxylate and Phenylboronic Acid in another window
• 4.2.4.1. Preparation of Chalcone and Its Further Robinson Annulation with Ethyl Acetoacetate p420-423 By Nuno R. Candeias Nuno R. Candeias Department of Chemistry and Bioengineering, Tampere University of Technology   Korkeakoulunkatu 8   Tampere   FI-33101 Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.4.1. Preparation of Chalcone and Its Further Robinson Annulation with Ethyl Acetoacetate in another window
• 4.1.1.9. Glycal Transformation into Surfactant 2-Deoxy Glycosides p247-251 By Catarina Dias ; Catarina Dias Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   C8, Piso 5, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Amélia P. Rauter Amélia P. Rauter Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   C8, Piso 5, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.9. Glycal Transformation into Surfactant 2-Deoxy Glycosides in another window
• 4.2.3.13. Enantioselective Synthesis and Derivatisation of 2-Hydroxy-1,2-diphenylethan-1-one p415-419 By Jonathan D. Sellars ; Jonathan D. Sellars Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar AnnMarie C. O’Donoghue ; AnnMarie C. O’Donoghue Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ian R. Baxendale ; Ian R. Baxendale Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar John M. Sanderson ; John M. Sanderson Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elizabeth J. Grayson Elizabeth J. Grayson Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.13. Enantioselective Synthesis and Derivatisation of 2-Hydroxy-1,2-diphenylethan-1-one in another window
• 5.1.1. Synthesis of Methyl Orange p448-450 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.1. Synthesis of Methyl Orange in another window
• 4.2.5.1. One-Pot Green Synthesis of Dihydropyran Heterocycles p428-431 By Dennis Russowsky ; Dennis Russowsky Laboratório de Síntese Organica K-210, Universidade Federal do Rio Grande do Sul, Instituto de Química   Av. Bento Gonçalves, 9500   CEP 91501-970   Porto Alegre   Rio Grande do Sul   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Camila S. Santos Camila S. Santos Laboratório de Síntese Organica K-210, Universidade Federal do Rio Grande do Sul, Instituto de Química   Av. Bento Gonçalves, 9500   CEP 91501-970   Porto Alegre   Rio Grande do Sul   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.1. One-Pot Green Synthesis of Dihydropyran Heterocycles in another window
• 4.2.5.2. Hantzsch Synthesis of Nifedipine p432-434 By Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences   Riccarton   Edinburgh EH14 4AS   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.2. Hantzsch Synthesis of Nifedipine in another window
• 4.1.1.10. Preparation of (1 R ,2 R ,3 R ,5 S )-(−)-Isopinocampheol Through a Hydroboration–Oxidation Reaction p252-256 By Marek P. Krzemiński Marek P. Krzemiński Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Toruń   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.10. Preparation of (1<em>R</em>,2<em>R</em>,3<em>R</em>,5<em>S</em>)-(−)-Isopinocampheol Through a Hydroboration–Oxidation Reaction in another window
• 5.1.5. Synthesis of 2-Nitro-4-methylaniline p462-464 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.5. Synthesis of 2-Nitro-4-methylaniline in another window
• 4.2.4.2. Conjugate Addition of Organocuprates to α,β-Unsaturated Ketones: Synthesis of 3,3-Dimethylcyclohexanone from 3-Methyl-2-cyclohexen-1-one p424-427 By Carlos Gregorio ; Carlos Gregorio Departamento de Química Orgánica, Facultad de Química, Universidad de Santiago de Compostela   Avda. Ciencias S/N   15782 Santiago de Compostela   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar F. Javier Sardina ; F. Javier Sardina Departamento de Química Orgánica, Facultad de Química, Universidad de Santiago de Compostela   Avda. Ciencias S/N   15782 Santiago de Compostela   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Antonio Mouriño Antonio Mouriño Departamento de Química Orgánica, Facultad de Química, Universidad de Santiago de Compostela   Avda. Ciencias S/N   15782 Santiago de Compostela   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.4.2. Conjugate Addition of Organocuprates to α,β-Unsaturated Ketones: Synthesis of 3,3-Dimethylcyclohexanone from 3-Methyl-2-cyclohexen-1-one in another window
• 4.1.2.1. Synthesis of Fructone p257-260 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry   Highfield, Southampton   Hampshire   SO17 1BJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.1. Synthesis of Fructone in another window
• 5.1.6. Synthesis of 1-Nitronaphthalene p465-467 By Adam Dzielendziak Adam Dzielendziak Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Torun   87-100 Torun   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.6. Synthesis of 1-Nitronaphthalene in another window
• 5.1.4. Regioselectivity in the Nitration of Acylanilines by Electrophilic Aromatic Substitution p456-461 By João P. Telo ; João P. Telo CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro P. Santos ; Pedro P. Santos CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar João V. Moreira ; João V. Moreira CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mariana L. Santos ; Mariana L. Santos CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana T. Batista Ana T. Batista CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.4. Regioselectivity in the Nitration of Acylanilines by Electrophilic Aromatic Substitution in another window
• 5.1.3. Synthesis of 2-(2,4-Dinitrobenzyl)pyridine p454-455 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.3. Synthesis of 2-(2,4-Dinitrobenzyl)pyridine in another window
• 5.1.2. Halogenation Reactions of Vanillin p451-453 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nigel P. Botting ; Nigel P. Botting School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Brian A. Chalmers ; Brian A. Chalmers School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Iain L. J. Patterson Iain L. J. Patterson School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.2. Halogenation Reactions of Vanillin in another window
• 5.2.2. Synthesis of 4,4′-Di- tert -butylbiphenyl p480-481 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.2. Synthesis of 4,4′-Di-<em>tert</em>-butylbiphenyl in another window
• 5.2.4. Synthesis of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin p485-489 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando M. J. Domingues ; Fernando M. J. Domingues Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. S. R. O. Rocha ; Graça M. S. R. O. Rocha Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria da Graça ; Maria da Graça Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar P. M. S. Neves ; P. M. S. Neves Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria do Amparo F. Faustino ; Maria do Amparo F. Faustino Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.4. Synthesis of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin in another window
• 5.2.7. Synthesis of Musk Ketone p496-499 By João Paulo Telo João Paulo Telo CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.7. Synthesis of Musk Ketone in another window
• 5.2.6. Synthesis of 3-Bromo-7-ethylcarbamate-4-methylcoumarin p493-495 By Paula S. Branco ; Paula S. Branco Departamento de Química, Faculdade de Ciências e Tecnologia, UNL   2829-516 Caparica   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Maria Lourenço Ana Maria Lourenço Departamento de Química, Faculdade de Ciências e Tecnologia, UNL   2829-516 Caparica   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.6. Synthesis of 3-Bromo-7-ethylcarbamate-4-methylcoumarin in another window
• 5.2.1. Synthesis of 1,4-Di- t -butyl-2,5-dimethoxybenzene p477-479 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.1. Synthesis of 1,4-Di-<em>t</em>-butyl-2,5-dimethoxybenzene in another window
• 4.2.5.5. A Multicomponent Reaction of Isocyanides for the Synthesis of 4-Chromanone-2-carboxamides p443-447 By Ana G. Neo ; Ana G. Neo Departamento de Química Orgánica e Inorgánica, F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jesús Díaz ; Jesús Díaz Departamento de Química Orgánica e Inorgánica, F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos F. Marcos Carlos F. Marcos Departamento de Química Orgánica e Inorgánica, F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.5. A Multicomponent Reaction of Isocyanides for the Synthesis of 4-Chromanone-2-carboxamides in another window
• 5.2.3. Synthesis of a Macrocycle: C -Methyl[4]resorcinarene p482-484 By Christopher Baker ; Christopher Baker School of Pharmacy and Biomolecular Sciences, University of Brighton   Huxley Building   Brighton BN2 4GJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexander S. Cragg ; Alexander S. Cragg School of Pharmacy and Biomolecular Sciences, University of Brighton   Huxley Building   Brighton BN2 4GJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Raghuram R. Kothur ; Raghuram R. Kothur School of Pharmacy and Biomolecular Sciences, University of Brighton   Huxley Building   Brighton BN2 4GJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Flavia Fucassi ; Flavia Fucassi School of Pharmacy and Biomolecular Sciences, University of Brighton   Huxley Building   Brighton BN2 4GJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Peter J. Cragg Peter J. Cragg School of Pharmacy and Biomolecular Sciences, University of Brighton   Huxley Building   Brighton BN2 4GJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.3. Synthesis of a Macrocycle: <em>C</em>-Methyl[4]resorcinarene in another window
• 5.2.9. Synthesis of Eosin p504-507 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.9. Synthesis of Eosin in another window
• 4.2.5.4. Preparation of Phenylglycine and Hydroxymorpholine Derivatives Through a Petasis Borono–Mannich Reaction p439-442 By Nuno R. Candeias ; Nuno R. Candeias Department of Chemistry and Bioengineering, Tampere University of Technology   Korkeakoulunkatu 8   Tampere   FI-33101 Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Roberta Paterna ; Roberta Paterna Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro M. S. D. Cal ; Pedro M. S. D. Cal Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro M. P. Gois Pedro M. P. Gois Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.4. Preparation of Phenylglycine and Hydroxymorpholine Derivatives Through a Petasis Borono–Mannich Reaction in another window
• 4.2.5.3. A Ugi Multicomponent Reaction in the Synthesis of N -Cyclohexyl-2-[ N -(4-methoxybenzyl)acetamide]-2-(thien-2-yl)acetamide p435-438 By Susana P. G. Costa ; Susana P. G. Costa University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Manuela M. Raposo ; M. Manuela M. Raposo University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cátia I. C. Esteves Cátia I. C. Esteves University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.3. A Ugi Multicomponent Reaction in the Synthesis of <em>N</em>-Cyclohexyl-2-[<em>N</em>-(4-methoxybenzyl)acetamide]-2-(thien-2-yl)acetamide in another window
• 4.1.2.2. Synthesis of Flavone p261-263 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.2. Synthesis of Flavone in another window
• 5.2.10. Synthesis and Formylation of 5-Piperidino-2,2′-bithiophene p508-513 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.10. Synthesis and Formylation of 5-Piperidino-2,2′-bithiophene in another window
• 6.2. Synthesis of the Antitumoral Drug 2,4,6-Tris(dimethylamino)-1,3,5-triazine via Sequential Nucleophilic Substitution p535-538 By Filipa Siopa ; Filipa Siopa Instituto de Investigação, do Medicamento (iMed.ULisboa), Faculdade de Farmácia, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nuno Candeias ; Nuno Candeias Department of Chemistry and Bioengineering, Tampere University of Technology   Korkeakoulunkatu 8   Tampere   FI-33101   Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Instituto de Investigação, do Medicamento (iMed.ULisboa), Faculdade de Farmácia, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.2. Synthesis of the Antitumoral Drug 2,4,6-Tris(dimethylamino)-1,3,5-triazine <em>via</em> Sequential Nucleophilic Substitution in another window
• 5.2.5. Solventless Synthesis, Separation and Characterization of Zinc and Free-Base Tetraphenyl Porphyrin p490-492 By Waqar Rizvi ; Waqar Rizvi Hunter College of the City University of New York   695 Park Avenue   New York   New York 10065   USA The Graduate Center of the City University of New York   365 Fifth Avenue   New York   New York 10016   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Charles M. Drain ; Charles M. Drain Hunter College of the City University of New York   695 Park Avenue   New York   New York 10065   USA The Graduate Center of the City University of New York   365 Fifth Avenue   New York   New York 10016   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Patrick Moy ; Patrick Moy Hunter College of the City University of New York   695 Park Avenue   New York   New York 10065   USA Search for other works by this author on: This Site PubMed Google Scholar Matthew J. Jurow Matthew J. Jurow The Molecular Foundry, Lawrence Berkeley National Laboratory   Berkeley   California 94720   USA Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.5. Solventless Synthesis, Separation and Characterization of Zinc and Free-Base Tetraphenyl Porphyrin in another window
• 5.1.8. Preparation of p -Bromoaniline p472-476 By Abel J. S. C. Vieira Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.8. Preparation of <em>p</em>-Bromoaniline in another window
• 6.3. Benzotriazole, a Useful Synthetic Auxiliary in Heterocyclizations p539-541 By João Lavrado ; João Lavrado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marta Figueiras ; Marta Figueiras Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eduardo Ruivo ; Eduardo Ruivo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana Lucas ; Susana Lucas Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Paulo Alexandra Paulo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Pharmaceutical and Medicinal Chemistry Department, Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.3. Benzotriazole, a Useful Synthetic Auxiliary in Heterocyclizations in another window
• 5.1.7. Selective Boc-Protection and Bromination of Pyrazoles p468-471 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry, Highfield   Southampton   Hampshire   SO17 1BJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.7. Selective Boc-Protection and Bromination of Pyrazoles in another window
• 4.1.2.3. Synthesis and Characterisation of H 2 salen: An Introduction to 1D and 2D NMR Spectroscopy p264-268 By Maria J. Villa de Brito Maria J. Villa de Brito DQB, CQE, Faculdade de Ciências da Universidade de Lisboa   Campo Grande, 1749-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.3. Synthesis and Characterisation of H₂salen: An Introduction to 1D and 2D NMR Spectroscopy in another window
• 4.1.2.4. Synthesis of Lophine and Conversion into Dimers p269-271 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.4. Synthesis of Lophine and Conversion into Dimers in another window
• 6.4. Synthesis of 4,5-Dicyanobenzene-1,2-dithiol p542-544 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.4. Synthesis of 4,5-Dicyanobenzene-1,2-dithiol in another window
• 4.1.2.5. Synthesis of Dibenzalacetone 2,4-Dinitrophenylhydrazone p272-276 By Ana Margarida Madureira ; Ana Margarida Madureira Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Bela Santana ; Ana Bela Santana Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Emília Valente ; Emília Valente Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.5. Synthesis of Dibenzalacetone 2,4-Dinitrophenylhydrazone in another window
• 4.1.2.6. Synthesis and Structural Characterization of an Antitubercular Isoniazid Hydrazone p277-281 By Susana Santos ; Susana Santos Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   Ed. C8   Campo Grande, 1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Filomena Martins Filomena Martins Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   Ed. C8   Campo Grande, 1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.6. Synthesis and Structural Characterization of an Antitubercular Isoniazid Hydrazone in another window
• 7.3. Recycling Bromovanillin into Ferulic Acid-Based Antioxidants p559-563 By Tiago Silva ; Tiago Silva CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Daniel Chavarria ; Daniel Chavarria CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Lisa Sequeira ; Lisa Sequeira CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Rua do Campo Alegre s/n   4169-007   Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.3. Recycling Bromovanillin into Ferulic Acid-Based Antioxidants in another window
• 4.1.2.7. Preparation of a Tosylhydrazidyl N -Glycosyl Derivative of d -Glucuronic Acid via Tosylhydrazone Formation and Intramolecular Ring Closure p282-284 By Nuno M. Xavier Nuno M. Xavier Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.7. Preparation of a Tosylhydrazidyl <em>N</em>-Glycosyl Derivative of <span class="small-caps">d</span>-Glucuronic Acid <em>via</em> Tosylhydrazone Formation and Intramolecular Ring Closure in another window
• 7.4. Sonogashira Coupling Reaction of Aryl Derivatives: A Versatile Method for Acetylide Building Blocks p564-567 By Tiago J. Silva ; Tiago J. Silva Centro de Ciências Moleculares de Materiais, Faculdade de Ciências da Universidade de Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. Mendes ; Paulo J. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Évora   Portugal Search for other works by this author on: This Site PubMed Google Scholar António P. S. Teixeira ; António P. S. Teixeira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Évora   Portugal Search for other works by this author on: This Site PubMed Google Scholar M. Paula Robalo ; M. Paula Robalo Área Departamental de Engenharia Química, Instituto Superior de Engenharia de Lisboa   Portugal Centro de Química Estrutural, Complexo I, Instituto Superior Técnico, Universidade de Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar M. H. Garcia M. H. Garcia Centro de Ciências Moleculares de Materiais, Faculdade de Ciências da Universidade de Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.4. Sonogashira Coupling Reaction of Aryl Derivatives: A Versatile Method for Acetylide Building Blocks in another window
• 5.2.11. Synthesis of 3-Bromosalicylaldehyde by Ortho -formylation of 2-Bromophenol p514-516 By Trond Vidar Hansen ; Trond Vidar Hansen Department of Pharmaceutical Chemistry, School of Pharmacy, University of Oslo   PO Box 1068 Blindern   N-0316 Oslo   Norway   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Lars Skattebøl Lars Skattebøl Department of Chemistry, University of Oslo   PO Box 1033 Blindern   N-0315 Oslo   Norway Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.11. Synthesis of 3-Bromosalicylaldehyde by <em>Ortho</em>-formylation of 2-Bromophenol in another window
• 6.1. Synthesis of 2,3-Quinoxalinedithiol p532-534 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.1. Synthesis of 2,3-Quinoxalinedithiol in another window
• 5.2.12. Synthesis of Indolo[3,2- b ]quinolin-11-one by Acid-Catalysed Intramolecular Double Cyclization p517-521 By João Lavrado ; João Lavrado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Marta Figueiras ; Marta Figueiras Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar David M. Pereira ; David M. Pereira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Sofia A. Santos ; Sofia A. Santos Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira ; Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal Pharmaceutical and Medicinal Chemistry Department, Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Paulo Alexandra Paulo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal Pharmaceutical and Medicinal Chemistry Department, Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649 003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.12. Synthesis of Indolo[3,2-<em>b</em>]quinolin-11-one by Acid-Catalysed Intramolecular Double Cyclization in another window
• 4.1.3.1. Green Metrics in a Cyclocondensation Reaction p285-289 By Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Hélio G. Bonacorso Hélio G. Bonacorso Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.1. Green Metrics in a Cyclocondensation Reaction in another window
• 4.1.3.2. Synthesis of 1 H -Pyrazoles Using Ball Mill, Grinding and Conventional Thermal Heating p290-293 By Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilherme C. Paveglio ; Guilherme C. Paveglio Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Kelvis Longhi Kelvis Longhi Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria   97105-900   Santa Maria   RS   Brazil   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.2. Synthesis of 1<em>H</em>-Pyrazoles Using Ball Mill, Grinding and Conventional Thermal Heating in another window
• 5.2.8. Synthesis of Methyl 4-oxo-4-(thiophen-2-yl)butanoate p500-503 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.8. Synthesis of Methyl 4-oxo-4-(thiophen-2-yl)butanoate in another window
• 5.2.13. Mild and Fast Friedel–Crafts Acylation Over Zeolites p522-525 By A. F. Brigas ; A. F. Brigas Universidade do Algarve, Departamento de Química e Farmácia, Centro de Investigação em Química do Algarve (CIQA), Campus de Gambelas   8005-139 Faro   Portugal Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB)   C8, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar F. Martins ; F. Martins Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB)   C8, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar R. Elvas-Leitão ; R. Elvas-Leitão Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB)   C8, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Instituto Politécnico de Lisboa, Instituto Superior de Engenharia de Lisboa (ISEL), Área Departamental de Engenharia Química   Rua Conselheiro Emídio Navarro, 1   1959-007 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar B. S. Santos ; B. S. Santos Universidade de Coimbra, Departamento de Química   3004-535 Coimbra   Portugal Search for other works by this author on: This Site PubMed Google Scholar A. Martins ; A. Martins Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB)   C8, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Instituto Politécnico de Lisboa, Instituto Superior de Engenharia de Lisboa (ISEL), Área Departamental de Engenharia Química   Rua Conselheiro Emídio Navarro, 1   1959-007 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar N. Nunes N. Nunes Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB)   C8, Campo Grande   1749-016 Lisboa   Portugal   [email protected] Instituto Politécnico de Lisboa, Instituto Superior de Engenharia de Lisboa (ISEL), Área Departamental de Engenharia Química   Rua Conselheiro Emídio Navarro, 1   1959-007 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.13. Mild and Fast Friedel–Crafts Acylation Over Zeolites in another window
• 4.1.3.3. Organocatalytic Enantioselective Michael Addition of Thiophenol to Chalcone p294-297 By Mariola Zielińska-Błajet ; Mariola Zielińska-Błajet Department of Organic Chemistry, Faculty of Chemistry, Wrocław University of Technology   Wyb. Wyspiańskiego 27   50-370 Wrocław   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jacek Skarżewski Jacek Skarżewski Department of Organic Chemistry, Faculty of Chemistry, Wrocław University of Technology   Wyb. Wyspiańskiego 27   50-370 Wrocław   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.3. Organocatalytic Enantioselective Michael Addition of Thiophenol to Chalcone in another window
• 7.9. An Efficient Methodology for the Synthesis of the 3-Styryl Coumarin p584-587 By António Manuel D. R. L. Pereira ; António Manuel D. R. L. Pereira Departamento de Química, Escola de Ciências e Tecnologia, Universidade de Évora, Colégio Luís António Verney   Rua Romão Ramalho, N°   59 7000-671   Portugal Laboratório HERCULES, Universidade de Évora   Largo Marquês de Marialva, N°   8 7000-809 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sérgio Miguel A. Martins Sérgio Miguel A. Martins Laboratório HERCULES, Universidade de Évora   Largo Marquês de Marialva, N°   8 7000-809 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.9. An Efficient Methodology for the Synthesis of the 3-Styryl Coumarin in another window
• 7.5. Convergent Synthesis of a Suzuki Product p568-572 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry, Highfield   Southampton   Hampshire   SO17 1BJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.5. Convergent Synthesis of a Suzuki Product in another window
• 7.10. Sonogashira Coupling Between a Vinylic Halide and a Terminal Alkyne p588-591 By Carine Maaliki ; Carine Maaliki UFR Sciences et Techniques de Tours, Parc Grandmont, Bat Yves Chauvin   32 Av. Monge 37200 Tours   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jérôme Thibonnet Jérôme Thibonnet UFR Sciences et Techniques de Tours, Parc Grandmont, Bat Yves Chauvin   32 Av. Monge 37200 Tours   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.10. Sonogashira Coupling Between a Vinylic Halide and a Terminal Alkyne in another window
• 5.2.14. Reactivity Studies of 1-Propyl-2-(thiophen-2-yl)-1 H -pyrrole p526-531 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sara Sofia Marques Fernandes ; Sara Sofia Marques Fernandes University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria Cidália Rodrigues Castro Maria Cidália Rodrigues Castro University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.14. Reactivity Studies of 1-Propyl-2-(thiophen-2-yl)-1<em>H</em>-pyrrole in another window
• 7.6. Oxidative Heck Reaction at Room Temperature p573-576 By Rajiv T. Sawant ; Rajiv T. Sawant Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center   Box 574, SE-751 23   Uppsala   Sweden   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ashkan Fardost ; Ashkan Fardost Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center   Box 574, SE-751 23   Uppsala   Sweden   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luke R. Odell Luke R. Odell Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center   Box 574, SE-751 23   Uppsala   Sweden   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.6. Oxidative Heck Reaction at Room Temperature in another window
• 4.1.3.4. Stereoselective Synthesis of meso -1-Allyl-2,6-diphenylpiperidin-4-one p298-300 By Ana-Belén García Delgado ; Ana-Belén García Delgado Departamento de Química Orgánica e Inorgánica, Facultad de Químicas, Universidad de Oviedo   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Noelia Quiñones ; Noelia Quiñones Departamento de Química Orgánica e Inorgánica, Facultad de Químicas, Universidad de Oviedo   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar María-Paz Cabal María-Paz Cabal Departamento de Química Orgánica e Inorgánica, Facultad de Químicas, Universidad de Oviedo   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.4. Stereoselective Synthesis of <em>meso</em>-1-Allyl-2,6-diphenylpiperidin-4-one in another window
• 4.1.3.5. Synthesis of a Squarylium Cyanine Dye as Potential Photosensitizer for Photodynamic Therapy (PDT) p301-305 By Marlene L. F. M. Pacheco ; Marlene L. F. M. Pacheco Department of Chemistry and CQ-VR, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sofia F. P. Friães ; Sofia F. P. Friães Department of Chemistry and CQ-VR, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renato E. Boto ; Renato E. Boto CICS-UBI – Health Sciences Research Centre, University of Beira Interior   Av. Infante D. Henrique   6200-506 Covilhã   Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo Almeida ; Paulo Almeida CICS-UBI – Health Sciences Research Centre, University of Beira Interior   Av. Infante D. Henrique   6200-506 Covilhã   Portugal Search for other works by this author on: This Site PubMed Google Scholar Amélia M. Silva ; Amélia M. Silva Department of Biology and Environment and CITAB, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal Search for other works by this author on: This Site PubMed Google Scholar Lucinda V. Reis Lucinda V. Reis Department of Chemistry and CQ-VR, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.5. Synthesis of a Squarylium Cyanine Dye as Potential Photosensitizer for Photodynamic Therapy (PDT) in another window
• 4.2.1.1. The Effects of Stoichiometry and Starting Material on the Product Identity and Yield in Grignard Addition Reactions p306-311 By Jane Brock Greco ; Jane Brock Greco Department of Chemistry, Johns Hopkins University   3400 N. Charles St.   Baltimore   MD 21218   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eric Hill Eric Hill Department of Chemistry, Johns Hopkins University   3400 N. Charles St.   Baltimore   MD 21218   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.1. The Effects of Stoichiometry and Starting Material on the Product Identity and Yield in Grignard Addition Reactions in another window
• 7.7. Synthesis of 2-Methyl-1,1′-binaphthalene via Suzuki Cross-Coupling Reaction p577-580 By Javier Iglesias-Sigüenza ; Javier Iglesias-Sigüenza Departamento de Química Orgánica, Universidad de Sevilla   C/ Profesor García González, n°1   41012-Sevilla   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar David Monge ; David Monge Departamento de Química Orgánica, Universidad de Sevilla   C/ Profesor García González, n°1   41012-Sevilla   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elena Díez Elena Díez Departamento de Química Orgánica, Universidad de Sevilla   C/ Profesor García González, n°1   41012-Sevilla   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.7. Synthesis of 2-Methyl-1,1′-binaphthalene <em>via</em> Suzuki Cross-Coupling Reaction in another window
• 7.8. Green Synthesis of Aromatic Ketones: Decarboxylative Palladium Catalysis Under Microwave Irradiation p581-583 By Jonas Sävmarker ; Jonas Sävmarker Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center   Box 574, SE-751 23   Uppsala   Sweden   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ashkan Fardost ; Ashkan Fardost Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center   Box 574, SE-751 23   Uppsala   Sweden   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luke R. Odell Luke R. Odell Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center   Box 574, SE-751 23   Uppsala   Sweden   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.8. Green Synthesis of Aromatic Ketones: Decarboxylative Palladium Catalysis Under Microwave Irradiation in another window
• 6.5. Nucleophilic Aromatic Substitution Reactions in 3,6-Bis(3,5-dimethyl-1 H -pyrazol-1-yl)-1,2,4,5-tetrazine p545-549 By Tiago J. L. Silva ; Tiago J. L. Silva Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Campo Grande   1049-016 Campo Grande, Lisboa   Portugal Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Campo Grande   1049-016 Campo Grande, Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Campo Grande   1049-016 Campo Grande, Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.5. Nucleophilic Aromatic Substitution Reactions in 3,6-Bis(3,5-dimethyl-1<em>H</em>-pyrazol-1-yl)-1,2,4,5-tetrazine in another window
• 4.2.1.2. Synthesis of Methyl Triphenylmethyl Ether p312-315 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.2. Synthesis of Methyl Triphenylmethyl Ether in another window
• 4.2.1.3. Grignard-Like Reaction in Water p316-318 By João R. Vale ; João R. Vale iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.3. Grignard-Like Reaction in Water in another window
• 7.1. A Solvent-Free Ullmann Coupling: Synthesis of 2,2′-Dinitrobiphenyl p550-553 By Laurel Goj Habgood ; Laurel Goj Habgood Rollins College   1000 Holt Avenue, Box 2743   Winter Park   FL 32789   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Richard W. Gregor Richard W. Gregor Rollins College   1000 Holt Avenue, Box 2743   Winter Park   FL 32789   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.1. A Solvent-Free Ullmann Coupling: Synthesis of 2,2′-Dinitrobiphenyl in another window
• 4.2.1.4. Cram’s Rule – Diastereoselective Grignard Addition to 2-Phenylpropanal p319-321 By Laura M. Hancock ; Laura M. Hancock Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University   Staffordshire   ST5 5BG   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Michael G. Edwards ; Michael G. Edwards Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University   Staffordshire   ST5 5BG   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graeme R. Jones ; Graeme R. Jones Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University   Staffordshire   ST5 5BG   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Matthew O’Brien Matthew O’Brien Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University   Staffordshire   ST5 5BG   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.4. Cram’s Rule – Diastereoselective Grignard Addition to 2-Phenylpropanal in another window
• 7.2. Reactivity Studies for the Synthesis of 5-Phenylthiophene-2-carbaldehyde by a Suzuki–Miyaura Coupling p554-558 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana Paula Graça da Costa ; Susana Paula Graça da Costa University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rosa Maria Ferreira Batista ; Rosa Maria Ferreira Batista University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rosa Cristina Moutinho Ferreira Rosa Cristina Moutinho Ferreira University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.2. Reactivity Studies for the Synthesis of 5-Phenylthiophene-2-carbaldehyde by a Suzuki–Miyaura Coupling in another window
• 4.2.1.5. Preparation of (4 R ,5 R )-4,5-Bis(diphenylhydroxymethyl)-2,2-dimethyldioxolane ((−)-TADDOL) p322-326 By Naylil M. R. Capreti ; Naylil M. R. Capreti Institute of Chemistry, State University of Campinas   C.P. 6154   13083-970   Campinas   SP   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Igor D. Jurberg Igor D. Jurberg Institute of Chemistry, State University of Campinas   C.P. 6154   13083-970   Campinas   SP   Brazil   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.5. Preparation of (4<em>R</em>,5<em>R</em>)-4,5-Bis(diphenylhydroxymethyl)-2,2-dimethyldioxolane ((−)-TADDOL) in another window
• 4.2.1.6. Synthesis of ( S )-Diphenyl(pyrrolidin-2-yl)methanol p327-330 By David Monge ; David Monge Departamento de Química Orgánica, Universidad de Sevilla   C/ Prof. García González, no. 1   41012-Sevilla   Spain   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Javier Iglesias-Sigüenza ; Javier Iglesias-Sigüenza Departamento de Química Orgánica, Universidad de Sevilla   C/ Prof. García González, no. 1   41012-Sevilla   Spain   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elena Díez Elena Díez Departamento de Química Orgánica, Universidad de Sevilla   C/ Prof. García González, no. 1   41012-Sevilla   Spain   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.6. Synthesis of (<em>S</em>)-Diphenyl(pyrrolidin-2-yl)methanol in another window
• 4.2.2.1. Solvent-Free Aldol Condensation Reactions: Synthesis of Chalcone Derivatives p331-334 By Barbora Morra ; Barbora Morra Department of Chemistry, University of Toronto   Toronto   Ontario   Canada   M5S 3H6   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Connie Tang ; Connie Tang Department of Chemistry, University of Toronto   Toronto   Ontario   Canada   M5S 3H6   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jonathon Fossella Jonathon Fossella Department of Chemistry, University of Toronto   Toronto   Ontario   Canada   M5S 3H6   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.1. Solvent-Free Aldol Condensation Reactions: Synthesis of Chalcone Derivatives in another window
• 4.2.2.2. Synthesis of ( E )-Chalcones [( E )-1,3-diarylprop-2-en-1-ones] p335-338 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.2. Synthesis of (<em>E</em>)-Chalcones [(<em>E</em>)-1,3-diarylprop-2-en-1-ones] in another window
• 4.2.2.3. A Solvent-Free Approach for Chalcone Synthesis via an Aldol Reaction p339-341 By Sofia F. P. Friães ; Sofia F. P. Friães Department of Chemistry and CQ-VR, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renato E. Boto ; Renato E. Boto CICS-UBI – Health Sciences Research Centre, University of Beira Interior   Av. Infante D. Henrique   6200-506 Covilhã   Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo Almeida ; Paulo Almeida CICS-UBI – Health Sciences Research Centre, University of Beira Interior   Av. Infante D. Henrique   6200-506 Covilhã   Portugal Search for other works by this author on: This Site PubMed Google Scholar Amélia M. Silva ; Amélia M. Silva Department of Biology and Environment and CITAB, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal Search for other works by this author on: This Site PubMed Google Scholar Lucinda V. Reis Lucinda V. Reis Department of Chemistry and CQ-VR, UTAD   Quinta de Prados   5000-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.3. A Solvent-Free Approach for Chalcone Synthesis <em>via</em> an Aldol Reaction in another window
• 4.2.2.4. Preparation of Dibenzylideneacetone p342-344 By Abel J. S. C. Vieira Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.4. Preparation of Dibenzylideneacetone in another window
• 4.2.2.5. l -Proline Catalyzed Aldol Reaction of 4-Nitrobenzaldehyde with Acetone p345-347 By Fang Fang ; Fang Fang Department of Chemistry, South University of Science and Technology of China   Shenzhen   518055   People’s Republic of China   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Xin-Yuan Liu ; Xin-Yuan Liu Department of Chemistry, South University of Science and Technology of China   Shenzhen   518055   People’s Republic of China   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Bin Tan Bin Tan Department of Chemistry, South University of Science and Technology of China   Shenzhen   518055   People’s Republic of China   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.5. <span class="small-caps">l</span>-Proline Catalyzed Aldol Reaction of 4-Nitrobenzaldehyde with Acetone in another window
• 4.2.2.6. Preparation of a β -Nitrostyrene Derivative by the Henry Reaction: Comparison of a Conventional and a Microwave-Assisted Method p348-351 By Daniel Martins ; Daniel Martins CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar Joana Reis ; Joana Reis CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges ; Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar Nuno Milhazes Nuno Milhazes CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto   Portugal CESPU/Superior Institute of Health of Sciences – North   Rua Central de Gandra, 1317   4585-116   Gandra PRD   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.6. Preparation of a <em>β</em>-Nitrostyrene Derivative by the Henry Reaction: Comparison of a Conventional and a Microwave-Assisted Method in another window
• 4.2.2.7. Synthesis of Aurone Derivatives Through Acid-Catalysed Aldol Condensation p352-354 By Ana R. Duarte ; Ana R. Duarte Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marta P. Carrasco ; Marta P. Carrasco Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição Ana S. Ressurreição Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.7. Synthesis of Aurone Derivatives Through Acid-Catalysed Aldol Condensation in another window
• 4.2.2.8. Synthesis of Pyrazole Heterocycles p355-358 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry, Highfield   Southampton   Hampshire   SO17 1BJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.8. Synthesis of Pyrazole Heterocycles in another window
• 4.2.2.9. A Green Approach to 3-Carbonylchromones p359-362 By Ana Bornadiego ; Ana Bornadiego Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jesús Díaz ; Jesús Díaz Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana G. Neo ; Ana G. Neo Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos F. Marcos Carlos F. Marcos Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura   10071 Cáceres   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.9. A Green Approach to 3-Carbonylchromones in another window
• 4.2.2.10. Synthesis of Indigo and Dyeing Process p363-365 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.10. Synthesis of Indigo and Dyeing Process in another window
• 4.2.3.1. Knorr Pyrazole Synthesis of Edaravone p366-369 By Ana Paula Francisco ; Ana Paula Francisco Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição ; Ana S. Ressurreição Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria de Jesus Perry ; Maria de Jesus Perry Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes Francisca Lopes Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.1. Knorr Pyrazole Synthesis of Edaravone in another window
• 4.2.3.2. Greener Solvent Substitution in a Verley–Doebner Condensation p370-372 By Jonathon W. Moir ; Jonathon W. Moir Department of Chemistry, University of Toronto   80 St. George Street   Toronto   Ontario   Canada   M5S 3H6   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrew P. Dicks Andrew P. Dicks Department of Chemistry, University of Toronto   80 St. George Street   Toronto   Ontario   Canada   M5S 3H6   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.2. Greener Solvent Substitution in a Verley–Doebner Condensation in another window
• 4.2.3.3. Knorr Synthesis of Diethyl 3,5-Dimethyl-1 H -pyrrole-2,4-dicarboxylate p373-375 By M. Soledad Pino-González ; M. Soledad Pino-González Organic Chemistry Department, Faculty of Sciences, University of Málaga   29071 Málaga   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cristina García-Ruiz ; Cristina García-Ruiz Organic Chemistry Department, Faculty of Sciences, University of Málaga   29071 Málaga   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisco Sarabia ; Francisco Sarabia Organic Chemistry Department, Faculty of Sciences, University of Málaga   29071 Málaga   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Gregorio Torres Gregorio Torres Organic Chemistry Department, Faculty of Sciences, University of Málaga   29071 Málaga   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.3. Knorr Synthesis of Diethyl 3,5-Dimethyl-1<em>H</em>-pyrrole-2,4-dicarboxylate in another window
• 4.2.3.4. Synthesis of Coumarin-3-carboxylic Acid p376-379 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.4. Synthesis of Coumarin-3-carboxylic Acid in another window
• 4.2.3.5. Synthesis of Lipophilic Antioxidants Based on Natural Models p380-386 By Sofia Benfeito ; Sofia Benfeito CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar Tiago Silva ; Tiago Silva CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar Diogo Magalhães Silva ; Diogo Magalhães Silva CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar E. Manuela Garrido ; E. Manuela Garrido CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Porto   Portugal Department of Chemical Engineering, School of Engineering (ISEP), Polytechnic of Porto   Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges ; Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Porto   Portugal Search for other works by this author on: This Site PubMed Google Scholar Jorge Garrido Jorge Garrido CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Porto   Portugal Department of Chemical Engineering, School of Engineering (ISEP), Polytechnic of Porto   Porto   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.5. Synthesis of Lipophilic Antioxidants Based on Natural Models in another window
• 4.2.3.6. A Simple and Ecological Preparation of a Chromene-3-carboxamide Derivative p387-390 By Marta Costa ; Marta Costa Chemistry Department, University of Minho, Campus de Gualtar   4710 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Fernanda Proença M. Fernanda Proença Chemistry Department, University of Minho, Campus de Gualtar   4710 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.6. A Simple and Ecological Preparation of a Chromene-3-carboxamide Derivative in another window
• 4.2.3.7. Synthesis of a Biologically Active Oxazol-5(4 H )-One via Erlenmeyer–Plöchl Reaction p391-395 By Catarina A. B. Rodrigues ; Catarina A. B. Rodrigues Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José M. G. Martinho ; José M. G. Martinho Centro de Química-Física Molecular and IN-Institute of Nanoscience and Nanothecnology, Instituto Superior Técnico   Av. Rovisco Pais   1049-001 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.7. Synthesis of a Biologically Active Oxazol-5(4<em>H</em>)-One <em>via</em> Erlenmeyer–Plöchl Reaction in another window
• 8.1. Synthesis of Dulcin p592-594 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 8.1. Synthesis of Dulcin in another window
• 8.2. Microwave-Assisted Solid-Phase Synthesis of Hydantoins p595-599 By Isabelle Parrot ; Isabelle Parrot IBMM UMR 5247 CNRS-Université Montpellier 1 et 2, Faculté des Sciences   Pl. Eugène Bataillon   34 095 Montpellier Cedex 5   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilhem Chaubet Guilhem Chaubet IBMM UMR 5247 CNRS-Université Montpellier 1 et 2, Faculté des Sciences   Pl. Eugène Bataillon   34 095 Montpellier Cedex 5   France   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 8.2. Microwave-Assisted Solid-Phase Synthesis of Hydantoins in another window
• 9.1.1. Preparation of Cyclohexene p600-602 By Abel J. S. C. Vieira ; Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elvira M. S. M. Gaspar Elvira M. S. M. Gaspar Faculty of Sciences and Technology, Universidade Nova de Lisboa   2829-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.1. Preparation of Cyclohexene in another window
• 9.1.2. A Green Synthesis of 2,3-Dibromo-3-phenylpropionic Acid and the Use of Kinetic Studies to Probe into the Elimination Product When Treated with a Weak Base in Different Solvents p603-607 By Malcolm I. Stewart ; Malcolm I. Stewart CRL, University of Oxford   12 Mansfield Road   Oxford   OX1 3TA   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Craig D. Campbell Craig D. Campbell CRL, University of Oxford   12 Mansfield Road   Oxford   OX1 3TA   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.2. A Green Synthesis of 2,3-Dibromo-3-phenylpropionic Acid and the Use of Kinetic Studies to Probe into the Elimination Product When Treated with a Weak Base in Different Solvents in another window
• 9.1.3. Dehydration of Methylcyclohexanols p608-613 By Cornelis A. Van Walree ; Cornelis A. Van Walree Department of Chemistry, Utrecht University   Budapestlaan 4b   3584 CD   Utrecht   The Netherlands School of Chemical and Physical Sciences, Flinders University   GPO Box 2100   Adelaide 5001   Australia   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Stephan A. Jonker ; Stephan A. Jonker Department of Chemistry, Utrecht University   Budapestlaan 4b   3584 CD   Utrecht   The Netherlands Search for other works by this author on: This Site PubMed Google Scholar Veronica Kaats-Richters Veronica Kaats-Richters Department of Chemistry, Utrecht University   Budapestlaan 4b   3584 CD   Utrecht   The Netherlands Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.3. Dehydration of Methylcyclohexanols in another window
• 9.1.4. Synthesis of 5-Hydroxymethylfurfural (HMF) from Fructose as a Bioplatform Intermediate p614-616 By Svilen P. Simeonov ; Svilen P. Simeonov Research Institute for Medicines and Pharmaceuticals Sciences, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisbon   Portugal Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences   Acad. G. Bonchev str., bl.9   1113 Sofia   Bulgaria   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Research Institute for Medicines and Pharmaceuticals Sciences, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003   Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.4. Synthesis of 5-Hydroxymethylfurfural (HMF) from Fructose as a Bioplatform Intermediate in another window
• 9.2.1. Synthesis of trans -9-(2-Phenylethenyl)anthracene p617-619 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.1. Synthesis of <em>trans</em>-9-(2-Phenylethenyl)anthracene in another window
• 9.2.2. Synthesis of 4-Vinylbenzoic acid p620-622 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.2. Synthesis of 4-Vinylbenzoic acid in another window
• 9.2.3. Preparation of Nitrostilbenes by the Wittig Reaction p623-626 By Francisca Lopes ; Francisca Lopes Research Institute for Medicines (iMed. ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria de Jesus Perry ; Maria de Jesus Perry Research Institute for Medicines (iMed. ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Paula Francisco Ana Paula Francisco Research Institute for Medicines (iMed. ULisboa), Faculdade de Farmácia da, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.3. Preparation of Nitrostilbenes by the Wittig Reaction in another window
• 9.2.4. Building an Alkene Spacer by the Wittig Reaction: Synthesis of 4-[2-(4-Nitrophenyl)ethenyl]benzonitrile p627-630 By António P. S. Teixeira ; António P. S. Teixeira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Paula Robalo ; M. Paula Robalo Área Departamental de Engenharia Química, Instituto Superior de Engenharia de Lisboa   Rua Conselheiro Emídio Navarro, 1   1959-007 Lisboa   Portugal Centro de Química Estrutural, Complexo I, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais   1049-001 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo J. Mendes Paulo J. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.4. Building an Alkene Spacer by the Wittig Reaction: Synthesis of 4-[2-(4-Nitrophenyl)ethenyl]benzonitrile in another window
• 9.2.5. Preparation of trans , trans -Distyrylbenzene by a Wittig Reaction p631-634 By Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences   Riccarton   Edinburgh EH14 4AS   United Kingdom   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.5. Preparation of <em>trans</em>,<em>trans</em>-Distyrylbenzene by a Wittig Reaction in another window
• 9.2.6. Synthesis and Reactivity of Phosphorus Ylides p635-639 By Ana Lúcia Cardoso ; Ana Lúcia Cardoso Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria I. L. Soares ; Maria I. L. Soares Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana M. M. Lopes ; Susana M. M. Lopes Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Teresa M. V. D. Pinho e Melo Teresa M. V. D. Pinho e Melo Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.6. Synthesis and Reactivity of Phosphorus Ylides in another window
• 9.2.7. Synthesis of 4-(Thiophen-2-yl)pyrrolidin-2-one via Horner–Wadsworth–Emmons Reaction and Reductive Cyclisation p640-645 By Jonathan D. Sellars ; Jonathan D. Sellars Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar AnnMarie C. O’Donoghue ; AnnMarie C. O’Donoghue Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ian R. Baxendale ; Ian R. Baxendale Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar John M. Sanderson ; John M. Sanderson Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elizabeth J. Grayson Elizabeth J. Grayson Chemistry Department, University of Durham   South Road   Durham   DH1 3LE   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.7. Synthesis of 4-(Thiophen-2-yl)pyrrolidin-2-one <em>via</em> Horner–Wadsworth–Emmons Reaction and Reductive Cyclisation in another window
• 9.3.1. A Guided-Inquiry Approach to Ring-Closing Metathesis p646-649 By Hala G. Schepmann ; Hala G. Schepmann Southern Oregon University   1250 Siskiyou Boulevard   Ashland   Oregon   97520   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Michelle Mynderse Michelle Mynderse 2371 Henley Avenue   Berkley   Michigan   48072   USA Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.3.1. A Guided-Inquiry Approach to Ring-Closing Metathesis in another window
• 9.3.2. Sequential Pd-Catalyzed Allylic Alkylation/Ru-Catalyzed Ring-Closing Metathesis p650-655 By Mélanie M. Lorion ; Mélanie M. Lorion UPMC Univ Paris 06, IPCM UMR CNRS 8232, FR2769, Institut Parisien de Chimie Moléculaire   Paris   France CNRS, UMR 8232   F-75005   Paris   France   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Claire Kammerer ; Claire Kammerer Search for other works by this author on: This Site PubMed Google Scholar Guillaume Prestat ; Guillaume Prestat Search for other works by this author on: This Site PubMed Google Scholar Giovanni Poli Giovanni Poli UPMC Univ Paris 06, IPCM UMR CNRS 8232, FR2769, Institut Parisien de Chimie Moléculaire   Paris   France CNRS, UMR 8232   F-75005   Paris   France   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.3.2. Sequential Pd-Catalyzed Allylic Alkylation/Ru-Catalyzed Ring-Closing Metathesis in another window
• 10.1. Diels–Alder Reaction of N -Phenylmaleimide with In situ Generated Buta-1,3-diene p656-659 By Artur M. S. Silva ; Artur M. S. Silva Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Department of Chemistry and QOPNA, University of Aveiro   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.1. Diels–Alder Reaction of <em>N</em>-Phenylmaleimide with <em>In situ</em> Generated Buta-1,3-diene in another window
• 10.2. Synthesis of Isomeric Bicyclopropyls from Conjugated Dienes p660-663 By Leiv K. Sydnes ; Leiv K. Sydnes Department of Chemistry   Allégt. 41   5007 Bergen   Norway   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Magne O. Sydnes Magne O. Sydnes Faculty of Science and Technology, Department of Mathematics and Natural Science   4036 Stavanger   Norway Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.2. Synthesis of Isomeric Bicyclopropyls from Conjugated Dienes in another window
• 10.3. Diels–Alder Reaction Between p -Benzoquinone and Cyclopentadiene and Subsequent Photochemical [2π + 2π] Cycloaddition p664-667 By Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences   Riccarton, Edinburgh EH14 4AS   United Kingdom   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.3. Diels–Alder Reaction Between <em>p</em>-Benzoquinone and Cyclopentadiene and Subsequent Photochemical [2π + 2π] Cycloaddition in another window
• 10.4. Click Chemistry p668-670 By Susana Dias Lucas ; Susana Dias Lucas Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eduardo F. P. Ruivo ; Eduardo F. P. Ruivo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marta Figueiras ; Marta Figueiras Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar João P. Lavrado ; João P. Lavrado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.4. Click Chemistry in another window
• 10.5. On-Water Synthesis of a Dipyrromethane via Bis-hetero-Diels–Alder Reaction of an Azoalkene with Pyrrole p671-675 By Susana M. M. Lopes ; Susana M. M. Lopes Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria I. L. Soares ; Maria I. L. Soares Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Lúcia Cardoso ; Ana Lúcia Cardoso Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Américo Lemos ; Américo Lemos CIQA, FCT, University of Algarve, Campus de Gambelas   8005-139 Faro   Portugal Search for other works by this author on: This Site PubMed Google Scholar Teresa M. V. D. Pinho e Melo Teresa M. V. D. Pinho e Melo Department of Chemistry, University of Coimbra   Rua Larga   3004-535 Coimbra   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.5. On-Water Synthesis of a Dipyrromethane <em>via</em> Bis-hetero-Diels–Alder Reaction of an Azoalkene with Pyrrole in another window
• 10.6. Application of 2,4,6-Trioxo-pyrimidin-5-ylidene Alditol in the Synthesis of Pyrano[2,3- d ]pyrimidine Containing a Sugar Moiety by Hetero-Diels–Alder Reaction p676-680 By Aleksandra Pałasz ; Aleksandra Pałasz Department of Organic Chemistry, Faculty of Chemistry, Jagiellonian University   Ingardena 3 St   30-060 Kraków   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dariusz Cież Dariusz Cież Department of Organic Chemistry, Faculty of Chemistry, Jagiellonian University   Ingardena 3 St   30-060 Kraków   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.6. Application of 2,4,6-Trioxo-pyrimidin-5-ylidene Alditol in the Synthesis of Pyrano[2,3-<em>d</em>]pyrimidine Containing a Sugar Moiety by Hetero-Diels–Alder Reaction in another window
• 10.7. Synthesis of a Spiroisoxazoline Oxindole by 1,3-Dipolar Cycloaddition p681-684 By Carlos J. A. Ribeiro ; Carlos J. A. Ribeiro Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira ; Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria M. M. Santos Maria M. M. Santos Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.7. Synthesis of a Spiroisoxazoline Oxindole by 1,3-Dipolar Cycloaddition in another window
• 10.8. Oxonitriles: Four-Step Ozonolysis, Aldol, Conjugate Addition, and Enolate Acylation Sequence p685-689 By Jesus A. Lujan-Montelongo ; Jesus A. Lujan-Montelongo Departamento de Química, Centro de Investigación y de Estudios Avanzados (Cinvestav), Avenida Instituto Politécnico Nacional 2508   San Pedro Zacatenco 07360   México D. F.   Mexico Search for other works by this author on: This Site PubMed Google Scholar Fraser F. Fleming Fraser F. Fleming Department of Chemistry, Drexel University   32 South 32nd St.   Philadelphia   PA 19104   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.8. Oxonitriles: Four-Step Ozonolysis, Aldol, Conjugate Addition, and Enolate Acylation Sequence in another window
• 10.9. Flash Vacuum Pyrolysis of o -Phenylene Sulfite: Formation and Purification of Cyclopentadienone Dimer p690-693 By R. Alan Aitken ; R. Alan Aitken EaStCHEM School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline E. R. Horsburgh Caroline E. R. Horsburgh EaStCHEM School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.9. Flash Vacuum Pyrolysis of <em>o</em>-Phenylene Sulfite: Formation and Purification of Cyclopentadienone Dimer in another window
• 11.1. Synthesis of 4-Methoxymethylbenzoic Acid p694-696 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 11.1. Synthesis of 4-Methoxymethylbenzoic Acid in another window
• 11.2. Synthesis of Benzopinacolone via Benzophenone Photoreduction Followed by Pinacol Rearrangement p697-700 By Filipa Siopa ; Filipa Siopa iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal   [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal   [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 11.2. Synthesis of Benzopinacolone <em>via</em> Benzophenone Photoreduction Followed by Pinacol Rearrangement in another window
• 11.3. Iodosulfonylation–Dehydroiodination of Styrene: Synthesis of ( E )-β-Tosylstyrene p701-703 By Carmen Nájera ; Carmen Nájera Departamento de Química Orgánica and Centro de Innovación en Química Avanzada (ORFEO-CINQA). Universidad de Alicante   Ctra. San Vicente s/n   E-03690-San Vicente del Raspeig (Alicante)   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José M. Sansano ; José M. Sansano Departamento de Química Orgánica and Centro de Innovación en Química Avanzada (ORFEO-CINQA). Universidad de Alicante   Ctra. San Vicente s/n   E-03690-San Vicente del Raspeig (Alicante)   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Miguel Yus Miguel Yus Departamento de Química Orgánica and Centro de Innovación en Química Avanzada (ORFEO-CINQA). Universidad de Alicante   Ctra. San Vicente s/n   E-03690-San Vicente del Raspeig (Alicante)   Spain   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 11.3. Iodosulfonylation–Dehydroiodination of Styrene: Synthesis of (<em>E</em>)-β-Tosylstyrene in another window
• 12.1.1. Aerobic Alcohol Oxidation Using a Cu( i )/TEMPO Catalyst System p704-708 By Nicholas J. Hill ; Nicholas J. Hill Department of Chemistry, University of Wisconsin-Madison   1101 University Avenue   Madison   WI   53706   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jessica M. Hoover ; Jessica M. Hoover Department of Chemistry, University of Wisconsin-Madison   1101 University Avenue   Madison   WI   53706   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Shannon S. Stahl Shannon S. Stahl Department of Chemistry, University of Wisconsin-Madison   1101 University Avenue   Madison   WI   53706   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.1. Aerobic Alcohol Oxidation Using a Cu(<span class="small-caps">i</span>)/TEMPO Catalyst System in another window
• 12.1.2. Chemoselective Oxidation of 1,2-Tetradecanediol p709-712 By Siedlecka Renata ; Siedlecka Renata Faculty of Chemistry, Organic Chemistry Department, Wroclaw University of Technology   Wyb. Wyspianskiego 27   50-370 Wroclaw   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Skarżewski Jacek Skarżewski Jacek Faculty of Chemistry, Organic Chemistry Department, Wroclaw University of Technology   Wyb. Wyspianskiego 27   50-370 Wroclaw   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.2. Chemoselective Oxidation of 1,2-Tetradecanediol in another window
• 12.1.3. Catalyzed Oxidation of Naphthalene to 1,4-Naphthoquinone p713-715 By Jacek Skarżewski Jacek Skarżewski Department of Organic Chemistry, Wroclaw University of Technology   Wyb. Wyspianskiego 27   50-370 Wroclaw   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.3. Catalyzed Oxidation of Naphthalene to 1,4-Naphthoquinone in another window
• 12.1.4. Alcohol Oxidation: Menthone Preparation by Menthol Oxidation Using Pyridinium Chlorochromate Immobilized in Silica Gel p716-719 By Rafael F. A. Gomes ; Rafael F. A. Gomes iMed.UL, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculty of Pharmacy, University of Lisbon   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.4. Alcohol Oxidation: Menthone Preparation by Menthol Oxidation Using Pyridinium Chlorochromate Immobilized in Silica Gel in another window
• 12.1.5. Heterocyclic Target Synthesis – Three-Step Syntheses from Benzaldehyde p720-724 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nigel P. Botting ; Nigel P. Botting School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Brian A. Chalmers ; Brian A. Chalmers School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrew D. Harper ; Andrew D. Harper School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Iain L. J. Patterson Iain L. J. Patterson School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.5. Heterocyclic Target Synthesis – Three-Step Syntheses from Benzaldehyde in another window
• 12.1.6. Oxidation of Activated Phenols p725-729 By Luísa M. Ferreira ; Luísa M. Ferreira LAQV, REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   Campus da Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paula S. Branco Paula S. Branco LAQV, REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   Campus da Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.6. Oxidation of Activated Phenols in another window
• 12.2.1. Synthesis of 2-(5-Phenylthien-2′-yl)benzothiazole p730-732 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana Paula Graça da Costa ; Susana Paula Graça da Costa Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rosa Maria Ferreira Batista Rosa Maria Ferreira Batista Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.1. Synthesis of 2-(5-Phenylthien-2′-yl)benzothiazole in another window
• 12.2.2. Synthesis of N - tert -butyloxycarbonyl-[2-(thien-2′-yl)benzoxazol-5-yl]- l -alanine methyl ester p733-736 By Susana P. G. Costa ; Susana P. G. Costa Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Manuela M. Raposo ; M. Manuela M. Raposo Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cátia I. C. Esteves ; Cátia I. C. Esteves Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar R. Cristina M. Ferreira R. Cristina M. Ferreira Department of Chemistry, University of Minho   Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.2. Synthesis of <em>N</em>-<em>tert</em>-butyloxycarbonyl-[2-(thien-2′-yl)benzoxazol-5-yl]-<span class="small-caps">l</span>-alanine methyl ester in another window
• 12.2.3. Synthesis of Flavones (2-Aryl-4 H -chromen-4-ones) p737-740 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department & QOPNA, University of Aveiro   Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.3. Synthesis of Flavones (2-Aryl-4<em>H</em>-chromen-4-ones) in another window
• 12.2.4. Hantzsch Synthesis of 3,5-Diethoxycarbonyl-2,6-dimethylpyridine p741-744 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nigel P. Botting ; Nigel P. Botting School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Brian A. Chalmers ; Brian A. Chalmers School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Iain L. J. Patterson ; Iain L. J. Patterson School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catherine M. Schofield Catherine M. Schofield School of Chemistry, University of St Andrews   North Haugh, St Andrews   Fife   KY16 9ST   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.4. Hantzsch Synthesis of 3,5-Diethoxycarbonyl-2,6-dimethylpyridine in another window
• 12.2.5. An “Out-of-the-Box” Example in Heterocyclic Chemistry: Synthesis of 3,6-Bis-(3,5-dimethyl-1 H -pyrazol-1-yl)-1,2,4,5-tetrazine p745-749 By Tiago J. L. Silva ; Tiago J. L. Silva Centro de Química Estrutural, Faculdade de Ciências da, Universidade de Lisboa   Campo Grande, 1049-1016 Campo Grande, Lisboa   Portugal Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da, Universidade de Lisboa   Campo Grande, 1049-1016 Campo Grande, Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da, Universidade de Lisboa   Campo Grande, 1049-1016 Campo Grande, Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.5. An “Out-of-the-Box” Example in Heterocyclic Chemistry: Synthesis of 3,6-Bis-(3,5-dimethyl-1<em>H</em>-pyrazol-1-yl)-1,2,4,5-tetrazine in another window
• 12.3.1. Catalytic Epoxidation of cis -Cyclooctene with MTO( vii ) and Pyrazole p750-753 By Elisabete P. Carreiro ; Elisabete P. Carreiro Centro de Química de Évora, Institute for Research and Advanced Studies, University of Evora, Chemistry Department, School of Science and Technology   Rua Romão Ramalho, no. 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anthony J. Burke Anthony J. Burke Centro de Química de Évora, Institute for Research and Advanced Studies, University of Evora, Chemistry Department, School of Science and Technology   Rua Romão Ramalho, no. 59   7000-671 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.1. Catalytic Epoxidation of <em>cis</em>-Cyclooctene with MTO(<span class="small-caps">vii</span>) and Pyrazole in another window
• 12.3.2. Stereoselective Epoxidation of Cholesterol by m -Chloroperoxybenzoic Acid p754-757 By Maria de Jesus Perry ; Maria de Jesus Perry Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Paula Francisco ; Ana Paula Francisco Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição ; Ana S. Ressurreição Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes Francisca Lopes Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.2. Stereoselective Epoxidation of Cholesterol by <em>m</em>-Chloroperoxybenzoic Acid in another window
• 12.3.3. Green Oxidation of Organic Compounds Using Metalloporphyrins p758-761 By Rose A. Clark ; Rose A. Clark Department of Chemistry, Saint Francis University   Loretto   PA 15940   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anne E. Stock ; Anne E. Stock Department of Chemistry, Saint Francis University   Loretto   PA 15940   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Edward P. Zovinka Edward P. Zovinka Department of Chemistry, Saint Francis University   Loretto   PA 15940   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.3. Green Oxidation of Organic Compounds Using Metalloporphyrins in another window
• 12.3.4. Catalytic Epoxidation of Carbamazepine p762-765 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando M. J. Domingues ; Fernando M. J. Domingues Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. S. R. O. Rocha ; Graça M. S. R. O. Rocha Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria da Graça P. M. S. Neves ; Maria da Graça P. M. S. Neves Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria do Amparo F. Faustino ; Maria do Amparo F. Faustino Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.4. Catalytic Epoxidation of Carbamazepine in another window
• 12.3.5. Regioselective Epoxidation of Geraniol by VO(acac) 2 Immobilised in Polystyrene p766-768 By Ana I. Vicente ; Ana I. Vicente iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.5. Regioselective Epoxidation of Geraniol by VO(acac)₂ Immobilised in Polystyrene in another window
• 12.3.6. Organocatalysed trans -Dihydroxylation of Olefins p769-772 By Andreia A. Rosatella ; Andreia A. Rosatella iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.6. Organocatalysed <em>trans</em>-Dihydroxylation of Olefins in another window
• 12.4.1. Synthesis of 6-Nitrosaccharin p773-775 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.4.1. Synthesis of 6-Nitrosaccharin in another window
• 13.1. Reduction of a Ketone Using Sodium Borohydride. Control of a Reaction by TLC p776-780 By Luis Constantino ; Luis Constantino Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto   1649-003 Lisbon   Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto   1649-003 Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Emília Valente Emília Valente Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto   1649-003 Lisbon   Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.1. Reduction of a Ketone Using Sodium Borohydride. Control of a Reaction by TLC in another window
• 13.2. Regioselective Catalytic Transfer Hydrogenation of Citral p781-783 By Jaime A. S. Coelho ; Jaime A. S. Coelho iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.2. Regioselective Catalytic Transfer Hydrogenation of Citral in another window
• 13.3. Regioselective 1,2-Reduction of an α,β-Unsaturated Ketone. A Green Experiment p784-788 By M. Manuela A. Pereira M. Manuela A. Pereira REQUIMTE, Chemistry Department, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa   2827-516 Caparica   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.3. Regioselective 1,2-Reduction of an α,β-Unsaturated Ketone. A Green Experiment in another window
• 13.4. Reduction of Diphenyl Sulfoxide Catalyzed by the Dioxo-Molybdenum Complex MoO 2 Cl 2 (H 2 O) 2 p789-793 By Ana C. Fernandes ; Ana C. Fernandes Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais, 1   1049-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Tiago A. Fernandes Tiago A. Fernandes Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais, 1   1049-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.4. Reduction of Diphenyl Sulfoxide Catalyzed by the Dioxo-Molybdenum Complex MoO₂Cl₂(H₂O)₂ in another window
• 13.5. Synthesis of Allylic Esters by Reduction of Fructone Followed by Wittig Olefination p794-797 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry   Highfield, Southampton   Hampshire   SO17 1BJ   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.5. Synthesis of Allylic Esters by Reduction of Fructone Followed by Wittig Olefination in another window
• 13.6. Preparation of a Thia-Tetraaza Macrocyclic Compound Through a Dual-Step Synthesis p798-802 By Judite Costa ; Judite Costa Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar João Franco Machado ; João Franco Machado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Fátima Cabral M. Fátima Cabral Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa   Av. Professor Gama Pinto   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.6. Preparation of a Thia-Tetraaza Macrocyclic Compound Through a Dual-Step Synthesis in another window
• 13.7. Asymmetric Reduction of Acetophenone with Borane Catalyzed by B -Methoxy-oxazaborolidine p803-806 By Marek P. Krzemiński Marek P. Krzemiński Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus, University in Toruń   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.7. Asymmetric Reduction of Acetophenone with Borane Catalyzed by <em>B</em>-Methoxy-oxazaborolidine in another window
• 13.8. Synthesis of 4,5-Bis(benzoylthio)-1,3-dithiole-2-thione p807-810 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais   1, 1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais   1, 1049-001 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.8. Synthesis of 4,5-Bis(benzoylthio)-1,3-dithiole-2-thione in another window
• 13.9. Organocatalytic Asymmetric Reduction of ( E )- N ,1-Diphenyl-1-propanimine to N -(1-Phenylpropyl)aniline with Trichlorosilane p811-814 By Pedro Barrulas ; Pedro Barrulas Departamento de Química e Centro de Química de Évora, Universidade de Évora   Rua Romão Ramalho, 59   7000 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anthony Burke Anthony Burke Departamento de Química e Centro de Química de Évora, Universidade de Évora   Rua Romão Ramalho, 59   7000 Évora   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.9. Organocatalytic Asymmetric Reduction of (<em>E</em>)-<em>N</em>,1-Diphenyl-1-propanimine to <em>N</em>-(1-Phenylpropyl)aniline with Trichlorosilane in another window
• 14.1. Benzilic Acid Rearrangement p815-817 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro   5001-801 Vila Real   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.1. Benzilic Acid Rearrangement in another window
• 14.2. Preparation of Phenyl Acetate and Its Conversion into 4-Hydroxyacetophenone p818-820 By Eimíle Sheehy ; Eimíle Sheehy Center for Synthesis and Chemical Biology, School of Chemistry, University College Dublin   Dublin 4   Ireland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paul Evans Paul Evans Center for Synthesis and Chemical Biology, School of Chemistry, University College Dublin   Dublin 4   Ireland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.2. Preparation of Phenyl Acetate and Its Conversion into 4-Hydroxyacetophenone in another window
• 14.3. Multistep Synthesis of Dilantin p821-825 By Paula C. Castilho ; Paula C. Castilho CQM, Centro de Competências de Ciências Exactas e das Engenharias, Universidade da Madeira, Campus Universitário da Penteada   9020-105 Funchal   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro Ideia Pedro Ideia CQM, Centro de Competências de Ciências Exactas e das Engenharias, Universidade da Madeira, Campus Universitário da Penteada   9020-105 Funchal   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.3. Multistep Synthesis of Dilantin in another window
• 14.4. Preparation of Isoborneol Through the Wagner–Meerwein Rearrangement Reaction of (1 R )-(+)-Camphene p826-829 By Marek P. Krzemiński Marek P. Krzemiński Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Toruń   Poland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.4. Preparation of Isoborneol Through the Wagner–Meerwein Rearrangement Reaction of (1<em>R</em>)-(+)-Camphene in another window
• 14.5. Umbelliferone: A Natural Scaffold Suitable for the Synthesis of ortho -Acetylhydroxycoumarins via Fries Rearrangement Reaction p830-833 By Saleta Vazquez-Rodriguez ; Saleta Vazquez-Rodriguez CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria João Matos ; Maria João Matos CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eugenio Uriarte ; Eugenio Uriarte Department of Organic Chemistry, Faculty of Pharmacy, University of Santiago de Compostela   Spain Search for other works by this author on: This Site PubMed Google Scholar Lourdes Santana ; Lourdes Santana Department of Organic Chemistry, Faculty of Pharmacy, University of Santiago de Compostela   Spain Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.5. Umbelliferone: A Natural Scaffold Suitable for the Synthesis of <em>ortho</em>-Acetylhydroxycoumarins <em>via</em> Fries Rearrangement Reaction in another window
• 14.6. Preparation of 4,5-Functionalized Cyclopentenone via Cyclization of a Stenhouse Adduct p834-837 By Jaime A. S. Coelho ; Jaime A. S. Coelho iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003   Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.6. Preparation of 4,5-Functionalized Cyclopentenone <em>via</em> Cyclization of a Stenhouse Adduct in another window
• 14.7. Synthesis of a Chiral Salen. Examples of the Schmidt Rearrangement and Ultrasound Activation p838-840 By Maria Elisa da Silva Serra ; Maria Elisa da Silva Serra Department of Chemistry, University of Coimbra   Coimbra   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dina Maria Bairrada Murtinho Dina Maria Bairrada Murtinho Department of Chemistry, University of Coimbra   Coimbra   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.7. Synthesis of a Chiral Salen. Examples of the Schmidt Rearrangement and Ultrasound Activation in another window
• 15.1. Bioreduction of N -Oxide Moiety p841-846 By María Laura Lavaggi ; María Laura Lavaggi Laboratorio de Química Orgánica, Instituto de Química Biológica, Facultad de Ciencias, Universidad de la República   Iguá 4225   Montevideo 11400   Uruguay   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mercedes González ; Mercedes González Laboratorio de Química Orgánica, Instituto de Química Biológica, Facultad de Ciencias, Universidad de la República   Iguá 4225   Montevideo 11400   Uruguay   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Hugo Cerecetto Hugo Cerecetto Área de Radiofarmacia, Centro de Investigaciones Nucleares, Facultad de Ciencias, Universidad de la República   Mataojo 2055   Montevideo 11400   Uruguay   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 15.1. Bioreduction of <em>N</em>-Oxide Moiety in another window
• 16.1. Preparation of Nylon 6,6 by Interfacial Polymerization p847-848 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais   1649-003 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.1. Preparation of Nylon 6,6 by Interfacial Polymerization in another window
• 16.2. Synthesis of Copolymer from Acrylamide (AA), 2-Acrylamido-2-methylpropane-sulfonic Acid (AMPS) and N , N -Methyleno-bis-acrylamide (BA) p849-852 By Fátima Coelho ; Fátima Coelho Department of Chemistry, Instituto Superior Técnico, University of Lisbon, CERENA-Centro de Recursos Naturais e Ambiente   Av. Rovisco Pais, 1   1049-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural   Av. Rovisco Pais, 1   1049-001 Lisboa   Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.2. Synthesis of Copolymer from Acrylamide (AA), 2-Acrylamido-2-methylpropane-sulfonic Acid (AMPS) and <em>N</em>,<em>N</em>-Methyleno-bis-acrylamide (BA) in another window
• 16.3. Multi-Step Synthesis of Nylon from Cyclohexene p853-858 By Marisa G. Weaver ; Marisa G. Weaver University of California at Santa Barbara, Department of Chemistry & Biochemistry   9510, Santa Barbara   California   93106-9510   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Morgan J. Gainer Morgan J. Gainer University of California at Santa Barbara, Department of Chemistry & Biochemistry   9510, Santa Barbara   California   93106-9510   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.3. Multi-Step Synthesis of Nylon from Cyclohexene in another window
• 16.4. Copolymerisation of Styrene and Methyl Methacrylate: An Introduction to Radical Polymerisation and Monomer Reactivity Ratios p859-863 By Valeria Arrighi ; Valeria Arrighi Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences   Riccarton   Edinburgh EH14 4AS   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences   Riccarton   Edinburgh EH14 4AS   UK   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.4. Copolymerisation of Styrene and Methyl Methacrylate: An Introduction to Radical Polymerisation and Monomer Reactivity Ratios in another window
• 16.5. Polymerization of ε-Caprolactone Using a Ruthenium( ii ) Mixed Metallocene Catalyst p864-867 By Andreia Valente ; Andreia Valente Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Tiago J. L. Silva ; Tiago J. L. Silva Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Lisboa   Portugal   [email protected] Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Évora   Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Évora   Portugal Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.5. Polymerization of ε-Caprolactone Using a Ruthenium(<span class="small-caps">ii</span>) Mixed Metallocene Catalyst in another window
• 17.1. The Cannizzaro Reaction: Synthesis of p -Chlorobenzyl Alcohol and p -Chlorobenzoic Acid p868-870 By Marja Asp-Lehtinen Marja Asp-Lehtinen Department of Chemistry and Bioengineering, Tampere University of Technology   P.O. Box 541   33101 Tampere   Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.1. The Cannizzaro Reaction: Synthesis of <em>p</em>-Chlorobenzyl Alcohol and <em>p</em>-Chlorobenzoic Acid in another window
• 17.2. The Kemp Elimination in Water: A Laboratory Experiment for Introductory Organic Chemistry p871-874 By Caitlin Williamson ; Caitlin Williamson Department of Chemistry and Biochemistry, Wilfrid Laurier University   75 University Ave W.   Waterloo   Ontario   Canada   N2L 3C5   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Kenneth E. Maly ; Kenneth E. Maly Department of Chemistry and Biochemistry, Wilfrid Laurier University   75 University Ave W.   Waterloo   Ontario   Canada   N2L 3C5   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Stephen L. MacNeil Stephen L. MacNeil Department of Chemistry and Biochemistry, Wilfrid Laurier University   75 University Ave W.   Waterloo   Ontario   Canada   N2L 3C5   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.2. The Kemp Elimination in Water: A Laboratory Experiment for Introductory Organic Chemistry in another window
• 17.3. Synthesis of Veratronitrile p875-877 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.3. Synthesis of Veratronitrile in another window
• 17.4. Synthesis of Levulinic Acid from Sucrose p878-880 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais   1049-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.4. Synthesis of Levulinic Acid from Sucrose in another window
• 17.5. Synthesis of 1-(4-Bromophenyl)-1 H -pyrrole by the Clauson-Kaas Reaction p881-884 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria Cidália Rodrigues Castro ; Maria Cidália Rodrigues Castro University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sara Sofia Marques Fernandes Sara Sofia Marques Fernandes University of Minho, Department of Chemistry, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.5. Synthesis of 1-(4-Bromophenyl)-1<em>H</em>-pyrrole by the Clauson-Kaas Reaction in another window
• 17.6. Synthesis of the Manganese( iii ) Complex of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin p885-887 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando M. J. Domingues ; Fernando M. J. Domingues Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. S. R. O. Rocha ; Graça M. S. R. O. Rocha Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria da Graça P. M. S. Neves ; Maria da Graça P. M. S. Neves Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria do Amparo F. Faustino ; Maria do Amparo F. Faustino Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department, University of Aveiro, Campus de Santiago   3810-193 Aveiro   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.6. Synthesis of the Manganese(<span class="small-caps">iii</span>) Complex of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin in another window
• 17.7. Synthesis of 1,3-Dithienylbenzo[ c ]thiophene p888-892 By Tiago J. L. Silva ; Tiago J. L. Silva Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora   Rua Romão Ramalho 59   7000-671 Évora   Portugal Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.7. Synthesis of 1,3-Dithienylbenzo[<em>c</em>]thiophene in another window
• 17.8. Synthesis of 1-Propyl-2-(thiophen-2-yl)-1 H -pyrrole p893-897 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar   4710-057 Braga   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.8. Synthesis of 1-Propyl-2-(thiophen-2-yl)-1<em>H</em>-pyrrole in another window
• 17.9. Rhodium Carbene C–H Insertion in Water and Catalyst Reuse p898-902 By Nuno R. Candeias ; Nuno R. Candeias Tampere University of Technology, Department of Chemistry and Bioengineering   Korkeakoulunkatu 8   Tampere   FI-33101   Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro M. P. Gois ; Pedro M. P. Gois University of Lisbon, Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso University of Lisbon, Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy   Av. Prof. Gama Pinto   1649-003 Lisbon   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.9. Rhodium Carbene C–H Insertion in Water and Catalyst Reuse in another window
• 17.10. Determination of the C–C Bond Strength of Substituted Cyclopropanes and Cyclobutanes using Bomb Calorimetry p903-907 By Steffanie H. Liskey ; Steffanie H. Liskey Department of Chemistry, Virginia Tech   1040 Drillfield Drive, Blacksburg   VA 24061   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alan R. Esker ; Alan R. Esker Department of Chemistry, Virginia Tech   1040 Drillfield Drive, Blacksburg   VA 24061   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar J. M. Tanko J. M. Tanko Department of Chemistry, Virginia Tech   1040 Drillfield Drive, Blacksburg   VA 24061   USA   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.10. Determination of the C–C Bond Strength of Substituted Cyclopropanes and Cyclobutanes using Bomb Calorimetry in another window
• 18.1. Resolution of a Chiral Amine and Recovery of Unwanted Enantiomer by Racemization: Towards a Greener Industrial Process p908-913 By Pedro P. Santos ; Pedro P. Santos CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro F. Pinheiro Pedro F. Pinheiro CQE, Department of Chemical Engineering, IST, University of Lisbon   Av. Rovisco Pais   1649-003 Lisbon   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.1. Resolution of a Chiral Amine and Recovery of Unwanted Enantiomer by Racemization: Towards a Greener Industrial Process in another window
• 18.2. Synthesis of Racemic Phenylalanine Methyl Ester and its Kinetic Resolution Catalysed by α-Chymotrypsin p914-918 By Luca Banfi ; Luca Banfi Department of Chemistry and Industrial Chemistry, University of Genova   via Dodecaneso   31 16146 Genova   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renata Riva Renata Riva Department of Chemistry and Industrial Chemistry, University of Genova   via Dodecaneso   31 16146 Genova   Italy   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.2. Synthesis of Racemic Phenylalanine Methyl Ester and its Kinetic Resolution Catalysed by α-Chymotrypsin in another window
• 18.3. Lipase Catalyzed Kinetic Resolution of Racemic 1-Phenylethanol p919-922 By Otto Långvik ; Otto Långvik Johan Gadolin Process Chemistry Centre, Laboratory of Organic Chemistry, Åbo Akademi University   Piispankatu 8   FI-20500 Turku   Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Tiina Saloranta ; Tiina Saloranta Johan Gadolin Process Chemistry Centre, Laboratory of Organic Chemistry, Åbo Akademi University   Piispankatu 8   FI-20500 Turku   Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Reko Leino Reko Leino Johan Gadolin Process Chemistry Centre, Laboratory of Organic Chemistry, Åbo Akademi University   Piispankatu 8   FI-20500 Turku   Finland   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.3. Lipase Catalyzed Kinetic Resolution of Racemic 1-Phenylethanol in another window
• 18.4 Enzymatic Kinetic Resolution and Separation of sec -Alcohols Methodology Based on Fatty Esters p923-926 By Carlos M. Monteiro ; Carlos M. Monteiro iMed. ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nuno M. T. Lourenço ; Nuno M. T. Lourenço Department of Bioengineering, IBB – Institute for Biotechnology and Bioengineering, Centre for Biological and Chemical Engineering, Instituto Superior Técnico   1049-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed. ULisboa, Faculdade de Farmácia da Universidade de Lisboa   Av. Prof. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.4 Enzymatic Kinetic Resolution and Separation of <em>sec</em>-Alcohols Methodology Based on Fatty Esters in another window
• 18.5. Enzymatic Kinetic Resolution and Preparative Separation of Secondary Alcohols p927-930 By Nuno M. T. Lourenço ; Nuno M. T. Lourenço Instituto Superior Técnico, Universidade de Lisboa   Av. Rovisco Pais, 1   1049-001 Lisboa   Portugal   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos M. Monteiro ; Carlos M. Monteiro Faculdade de Farmácia, Universidade de Lisboa   Av. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Faculdade de Farmácia, Universidade de Lisboa   Av. Gama Pinto   1649-003 Lisboa   Portugal   [email protected]   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.5. Enzymatic Kinetic Resolution and Preparative Separation of Secondary Alcohols in another window
• 18.6. Catalyzed Resolution and Simultaneous Selective Crystallization p931-934 By Jaan Parve ; Jaan Parve Institute of Technology, University of Tartu   Nooruse 1   50411 Tartu   Estonia Search for other works by this author on: This Site PubMed Google Scholar Lauri Vares ; Lauri Vares Institute of Technology, University of Tartu   Nooruse 1   50411 Tartu   Estonia Search for other works by this author on: This Site PubMed Google Scholar Indrek Reile ; Indrek Reile National Institute of Chemical Physics and Biophysics   Akadeemia tee 23   12618 Tallinn   Estonia Search for other works by this author on: This Site PubMed Google Scholar Tõnis Pehk ; Tõnis Pehk National Institute of Chemical Physics and Biophysics   Akadeemia tee 23   12618 Tallinn   Estonia Search for other works by this author on: This Site PubMed Google Scholar Ly Villo ; Ly Villo Department of Chemistry, Tallinn University of Technology   Ehitajate tee 5   19086 Tallinn   Estonia   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Omar Parve Omar Parve Department of Chemistry, Tallinn University of Technology   Ehitajate tee 5   19086 Tallinn   Estonia   [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.6. Catalyzed Resolution and Simultaneous Selective Crystallization in another window
• Subject Index p935-951 Open the PDF Link PDF for Subject Index in another window

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