macroscale and microscale organic experiments sixth (7th) edition pdf

• Email Sign-Up

Macroscale and microscale organic experiments

By kenneth l. williamson.

• 0 Want to read
• 0 Currently reading
• 0 Have read

My Reading Lists:

Use this Work

Create a new list

My book notes.

My private notes about this edition:

Check nearby libraries

• Library.link

Buy this book

This edition doesn't have a description yet. Can you add one ?

Previews available in: English

Showing 1 featured edition. View all 1 editions?

Add another edition?

Book Details

Edition notes.

Includes index.

Classifications

The physical object, source records, community reviews (0).

• Created July 30, 2011
• 6 revisions

Wikipedia citation

Copy and paste this code into your Wikipedia page. Need help?

Macroscale and Microscale Organic Experiments, 7th Edition

Kenneth l. williamson, katherine m. masters.

Succeed in your organic laboratory course with MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS, Seventh Edition. This proven, authoritative manual emphasizes safety and features new themed Modules experiments with real world applications. Using the manual's mix of macroscale and microscale experiments, you'll gain the knowledge and confidence you need to perform a wide variety of experiments, as well as experience working with conventionally-sized glassware.

• Table of Contents
• Meet the Authors
• Supplements
• Related Products

1. Introduction. 2. Laboratory Safety, Courtesy, and Waste Disposal Techniques. 3. Melting Points and Boiling Points. 4. Recrystallization. 5. Distillation. 6. Steam Distillation, Vacuum Distillation, and Sublimation. 7. Extraction. 8. Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste. 9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments. 10. Gas Chromatography: Analysis of Alkene Isomers. 11. Infrared Spectroscopy. 12. Nuclear Magnetic Resonance Spectroscopy. 13. Mass Spectroscopy. 14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis. 15. Computational Chemistry Elimination, Substitution, and Addition. 16. The SN2 Reaction: 1-Bromobutane. 17. Nucleophilic Substitution Reactions of Alkyl Halides. 18. Radical Initiated Chlorination of 1-Chlorobutane. 19. Alkenes from Alcohols: Cyclohexene from Cyclohexanol. 20. Bromination and Debromination: Purification of Cholesterol. 21. Dichlorocarbene Oxidation and Reduction. 22. Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid. 23. The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent. 24. Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol. 25. Catalytic Hydrogenation. 26. Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis. 27. Epoxidation of Cholesterol. Aromatic Substitution and Elimination. 28. Nitration of Methyl Benzoate 29. Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry. 30. Alkylation of Mesitylene. 31. The Friedel-Crafts Reaction: Anthraquinone and Anthracene. 32. Friedel-Crafts Acylation of Ferrocene: Acetylferrocene. 33. Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical. 34. 1,2,3,4-Tetraphenylnaphthalene via Benzyne. 35. Triptycene via Benzyne Reactions of Aldehydes and Ketones. 36. Aldehydes and Ketones. 37. Dibenzalacetone by the Aldol Condensation. 38. Grignard Synthesis of Triphenylmethanol and Benzoic Acid. 39. The Wittig and Wittig-Horner Reactions Reactions of Carboxylic Acids, Esters, and Amines. 40. Esterification and Hydrolysis. 41. Acetylsalicylic Acid (Aspirin). 42. Malonic Ester of a Barbiturate. 43. Amines. 44. The Sandmeyer Reaction: 1-Bromo-4-chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene. 45. Synthesis and Bioessay of Sulfanilamide and Derivatives. 46. Dyes and Dyeing. 47. Martius Yellow. 48. Diels-Alder Reaction. 49. Ferrocene [Bis(cyclopentadienyl)iron]. 50. A Diels-Alder Reaction Puzzle: The Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride. 51. Tetraphenylcyclopentadienone. 52. Hexaphenylbenzene and Dimethyl Tetraphenylphthalate. Derivatives of 1,2-Diphenylethane: A Multistep Synthesis. 53. The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine. 54. Nitric Acid Oxidation; Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline. 55. Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil. 56. The Synthesis of 2,2-Dimethyl-1,5-dioxolane; The Acetonide Derivative of a Vicinal Diol. 57. The 1,4-Addition: Reductive Acetylation of Benzil. 58. Synthesis of an Alkyne from an Alkene; Bromination and Dehydrobromination: Stilbene and Diphenylacetylene. 59. The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid. 60. Multicomponent Reactions: The Aqueous Passerini Reaction. 61. Chemiluminescence: Syntheses of Cyalume and Luminol. 62. Photochemistry: The Synthesis of Benzopinacol Natural Product Chemistry and Biochemistry. 63. Carbohydrates and Sweeteners. 64. Virstatin, a Possible Treatment for Cholera. 65. Biosynthesis of Ethanol and Enzymatic Reactions. 66. The Synthesis of Natural Products: Pseudopellitierene and Camphor. 67. Polymers: Synthesis and Recycling. Agricultural Science Module: Technique of Distillation and Ester Synthesis Food Science Module: Techniques of Thin-Layer & Column Chromatography and an Isomerization Reaction Textile Module: Techniques of Recrystallization & Acid-Base Extraction and Synthesis of Methyl Orange Forensics Module: Two-Step Synthesis & Blood Detection 68. Searching the Chemical Literature.

Ken Williamson is retired from Mt. Holyoke College where he taught the organic chemistry laboratory course. He is an established authority on microscale techniques and regularly holds workshops and travels to campuses in the U.S., Canada, and Europe to demonstrate the use of microscale.

A PhD from Pennsylvania State University, Katherine Masters is director of the organic chemistry laboratory courses at Penn State.

New themed Module experiments include real life applications.

A related OWLv2 LabSkills course is available.

New themed Module experiments offer real life applications.

GREENER CHEMISTRY. Experiments that stress greener chemistry appear throughout the manual and are identified with a green chemistry icon. For example, the use of household bleach is explored as an alternative to the toxic chromium ion as an oxidizing agent for cyclohexanol.

AN EMPHASIS ON LABORATORY SAFETY. The laboratory safety chapter includes material on working with closed systems and laboratory courtesy.

A STRONG MASS SPECTROMETRY CHAPTER. The chapter on mass spectrometry describes time-of-flight and mass quadrupole analyzers and includes sections on GC-MS and computer-aided spectral identification, as well as ESI and MALDI ionization.

BIOASSAY EXPERIMENTS. The manual's bioassay experiments include a bioassay of eugenol isolated from cloves.

COMPREHENSIVE COVERAGE. Material is offered on diffuse reflectance IR analysis, capillary GC, and temperature programming.

PREMIUM WEBSITE. A Premium Website includes glassware-specific videos with pre-lab, gradable exercises.

Online Instructor's Resource Manual for Williamson/Masters' Macroscale and Microscale Organic Experiments, 7th 9781305884120

Enter the characters you see below

Sorry, we just need to make sure you're not a robot. For best results, please make sure your browser is accepting cookies.

Type the characters you see in this image:

Macroscale and Microscale Organic Experiments

7th Edition

eBook Features

• Read Anywhere Read your book anywhere, on any device, through RedShelf's cloud based eReader.
• Digital Notes and Study Tools Built-in study tools include highlights, study guides, annotations, definitions, flashcards, and collaboration.
• Text-to-Speech Compatible Have the book read to you!
• Offline Access ( 100% ) The publisher of this book allows a portion of the content to be used offline.
• Printing ( 20% ) The publisher of this book allows a portion of the content to be printed.
• Copy/Paste ( 20% ) The publisher of this book allows a portion of the content to be copied and pasted into external tools and documents.

This title is not available in your country.

Additional Book Details

Succeed in your organic laboratory course with MACROSCALE AND MICROSCALE ORGANIC EXPERIMENTS, Seventh Edition. This proven, authoritative manual emphasizes safety and features new themed Modules experiments with real world applications. Using the manual's mix of macroscale and microscale experiments, you'll gain the knowledge and confidence you need to perform a wide variety of experiments, as well as experience working with conventionally-sized glassware.

Select a Language

Macroscale and Microscale Organic Experiments, 7th Edition.

• MLA style: "Macroscale and Microscale Organic Experiments, 7th Edition.." The Free Library . 2017 Ringgold, Inc. 10 Aug. 2024 https://www.thefreelibrary.com/Macroscale+and+Microscale+Organic+Experiments%2c+7th+Edition.-a0491754784
• Chicago style: The Free Library . S.v. Macroscale and Microscale Organic Experiments, 7th Edition.." Retrieved Aug 10 2024 from https://www.thefreelibrary.com/Macroscale+and+Microscale+Organic+Experiments%2c+7th+Edition.-a0491754784
• APA style: Macroscale and Microscale Organic Experiments, 7th Edition.. (n.d.) >The Free Library. (2014). Retrieved Aug 10 2024 from https://www.thefreelibrary.com/Macroscale+and+Microscale+Organic+Experiments%2c+7th+Edition.-a0491754784

Terms of use | Privacy policy | Copyright © 2024 Farlex, Inc. | Feedback | For webmasters |

Macroscale and Microscale Organic Experiments 7th Edition

• Author(s) Kenneth Williamson
• Publisher Cengage Learning

Internet Archive Audio

• This Just In
• Grateful Dead
• Old Time Radio
• 78 RPMs and Cylinder Recordings
• Audio Books & Poetry
• Computers, Technology and Science
• Music, Arts & Culture
• News & Public Affairs
• Spirituality & Religion
• Radio News Archive

• Flickr Commons
• Occupy Wall Street Flickr
• NASA Images
• Solar System Collection
• Ames Research Center

• All Software
• Old School Emulation
• MS-DOS Games
• Historical Software
• Classic PC Games
• Software Library
• Kodi Archive and Support File
• Vintage Software
• CD-ROM Software
• CD-ROM Software Library
• Software Sites
• Tucows Software Library
• Shareware CD-ROMs
• Software Capsules Compilation
• CD-ROM Images
• ZX Spectrum
• DOOM Level CD

• Smithsonian Libraries
• FEDLINK (US)
• Lincoln Collection
• American Libraries
• Canadian Libraries
• Universal Library
• Project Gutenberg
• Children's Library
• Biodiversity Heritage Library
• Books by Language
• Additional Collections

• Prelinger Archives
• Democracy Now!
• Occupy Wall Street
• TV NSA Clip Library
• Animation & Cartoons
• Arts & Music
• Computers & Technology
• Cultural & Academic Films
• Ephemeral Films
• Sports Videos
• Videogame Videos
• Youth Media

Search the history of over 866 billion web pages on the Internet.

Mobile Apps

• Wayback Machine (iOS)
• Wayback Machine (Android)

Browser Extensions

Archive-it subscription.

• Explore the Collections
• Build Collections

Save Page Now

Capture a web page as it appears now for use as a trusted citation in the future.

Please enter a valid web address

• Donate Donate icon An illustration of a heart shape

Macroscale and microscale organic experiments

Bookreader item preview, share or embed this item, flag this item for.

• Graphic Violence
• Explicit Sexual Content
• Hate Speech
• Misinformation/Disinformation
• Marketing/Phishing/Advertising
• Misleading/Inaccurate/Missing Metadata

plus-circle Add Review comment Reviews

586 Previews

4 Favorites

DOWNLOAD OPTIONS

No suitable files to display here.

EPUB and PDF access not available for this item.

IN COLLECTIONS

Uploaded by AltheaB on September 26, 2011

SIMILAR ITEMS (based on metadata)